氧化铜膜阳极氧化方式对其形貌影响的研究

Q3 Engineering Eurasian Physical Technical Journal Pub Date : 2022-09-22 DOI:10.31489/2022no3/5-9
V. Smirnov
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引用次数: 0

摘要

本文介绍了单级电化学阳极氧化获得的Cu2O膜表面形貌的实验数据。该过程在恒定的50V外加电位和温度为13°C(90秒)的磷酸电解质中进行。在实验过程中,确定了最佳的合成参数。利用原子力显微镜对铜多孔膜的形貌进行了研究。研究了主要阳极氧化工艺参数对纳米多孔氧化Cu2O膜形貌的影响。根据实验工作的结果发现,根据阳极氧化工艺的参数,可以改变氧化铜的孔径,从几十纳米到几百微米,同时也可以改变膜的厚度。
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INVESTIGATION OF THE INFLUENCE OF ANODIZING MODES OF COPPER OXIDE FILMS ON THEIR MORPHOLOGY
This work presents experimental data on the surface morphology of Cu2O films obtained by single-stage electrochemical anodization. The process was carried out at a constant applied potential of 50V and at a temperature of 13°C (90 seconds) in an electrolyte based on phosphoric acid. During the experimental work, the optimal synthesis parameters were determined. The morphology of copper porous films was studied using atomic force microscopy Ntegra Therma. The effect of the main anodizing parameters on the morphology of the nanoporous Cu2O film was investigated. According to the results of experimental work, it was found that, depending on the parameters ofthe anodizing process, it is possible to vary the pore diameter of copper oxide from several tens of nanometersto hundreds of microns, while it is also possible to change the film thickness.
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