液相烧结LiTiZnMn铁氧体在辐射热和热条件下的初始磁导率研究

A. Surzhikov
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引用次数: 0

摘要

通过测量初始磁导率的温度依赖性,研究了锂钛铁氧体中的相转变和结构转变随时间、加热和冷却速率以及在热加热和辐射热加热下液相烧结温度的变化特征。以粉末混合物为原料,采用固相合成法合成了铁氧体。采用低熔点添加剂二氧化铋液相烧结制备铁氧体陶瓷。RT烧结是通过用脉冲(1.5–2.0)MeV电子束加热样品来进行的。已经确定,添加剂导致烧结铁氧体的缺陷状态较少,而辐射的作用在烧结的早期阶段增强了这种效果。建立了压实样品的加热和冷却速率对烧结铁氧体初始磁导率变化的影响规律。
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TUDY OF THE INITIAL MAGNETIC PERMEABILITY OF LiTiZnMnFERRITES OBTAINED BY LIQUID-PHASE SINTERING UNDER RADIATION-THERMAL AND THERMAL CONDITIONS
The measuring the temperature dependence of the initial permeability was used to study the features of phase and structural transformations in lithium-titanium ferrites as a function of time, heating and cooling rates, and the temperature of liquid-phase sintering under thermal and radiation-thermal heating. Ferrite was synthesized from powder mixture by solid-phase synthesis. A low-melting additive bismuth dioxide was used to obtain the ferrite ceramics by liquid-phase sintering. RT sintering was carried out by heating the samples with a pulsed (1.5–2.0) MeV electron beam. It was established that the additive leads to a less defective state of sintered ferrites, while the action of radiation enhances this effect in the early stages of sintering. The regularities of the influence of the heating and cooling rates of compacted samples on the change in the initial magnetic permeability of sintered ferrites are established.
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