{"title":"高纵横比微尺度硅孔阵列的深度反应离子刻蚀优化","authors":"Taeyeong Kim, Jungchul Lee","doi":"10.1186/s40486-022-00155-6","DOIUrl":null,"url":null,"abstract":"<div><p>During deep reactive ion etching (DRIE), microscale etch masks with small opening such as trenches or holes suffer from limited aspect ratio because diffusion of reactive ions and free radicals become progressively difficult as the number of DRIE cycle increases. For this reason, high aspect ratio structures of microscale trenches or holes are not readily available with standard DRIE recipes and microscale holes are more problematic than trenches due to omnidirectional confinement. In this letter, we propose an optimization for fabrication of high aspect ratio microscale hole arrays with an improved cross-sectional etch profile. Bias voltage and inductively coupled plasma power are considered as optimization parameters to promote the bottom etching of the high aspect ratio hole array. In addition, flow rates of octafluorocyclobutane (C<span>\\(_{4}\\)</span>F<span>\\(_{8}\\)</span>) and sulfur hexafluoride (SF<span>\\(_{6}\\)</span>) for passivation and depassivation steps, respectively, are considered as optimization parameters to reduce the etch undercut. As a result of optimization, the aspect ratio of 20 is achieved for 1.3 μm-diameter hole array and etch area reduction at the bottom relative to the top is improved to 21%.</p></div>","PeriodicalId":704,"journal":{"name":"Micro and Nano Systems Letters","volume":"10 1","pages":""},"PeriodicalIF":4.7000,"publicationDate":"2022-09-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://mnsl-journal.springeropen.com/counter/pdf/10.1186/s40486-022-00155-6","citationCount":"6","resultStr":"{\"title\":\"Optimization of deep reactive ion etching for microscale silicon hole arrays with high aspect ratio\",\"authors\":\"Taeyeong Kim, Jungchul Lee\",\"doi\":\"10.1186/s40486-022-00155-6\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>During deep reactive ion etching (DRIE), microscale etch masks with small opening such as trenches or holes suffer from limited aspect ratio because diffusion of reactive ions and free radicals become progressively difficult as the number of DRIE cycle increases. For this reason, high aspect ratio structures of microscale trenches or holes are not readily available with standard DRIE recipes and microscale holes are more problematic than trenches due to omnidirectional confinement. In this letter, we propose an optimization for fabrication of high aspect ratio microscale hole arrays with an improved cross-sectional etch profile. Bias voltage and inductively coupled plasma power are considered as optimization parameters to promote the bottom etching of the high aspect ratio hole array. In addition, flow rates of octafluorocyclobutane (C<span>\\\\(_{4}\\\\)</span>F<span>\\\\(_{8}\\\\)</span>) and sulfur hexafluoride (SF<span>\\\\(_{6}\\\\)</span>) for passivation and depassivation steps, respectively, are considered as optimization parameters to reduce the etch undercut. As a result of optimization, the aspect ratio of 20 is achieved for 1.3 μm-diameter hole array and etch area reduction at the bottom relative to the top is improved to 21%.</p></div>\",\"PeriodicalId\":704,\"journal\":{\"name\":\"Micro and Nano Systems Letters\",\"volume\":\"10 1\",\"pages\":\"\"},\"PeriodicalIF\":4.7000,\"publicationDate\":\"2022-09-09\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://mnsl-journal.springeropen.com/counter/pdf/10.1186/s40486-022-00155-6\",\"citationCount\":\"6\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Micro and Nano Systems Letters\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://link.springer.com/article/10.1186/s40486-022-00155-6\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q2\",\"JCRName\":\"NANOSCIENCE & NANOTECHNOLOGY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Micro and Nano Systems Letters","FirstCategoryId":"1085","ListUrlMain":"https://link.springer.com/article/10.1186/s40486-022-00155-6","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"NANOSCIENCE & NANOTECHNOLOGY","Score":null,"Total":0}
引用次数: 6
摘要
在深度反应离子蚀刻(DRIE)过程中,随着DRIE循环次数的增加,反应离子和自由基的扩散变得越来越困难,因此具有小开口的微尺度蚀刻掩膜(如沟槽或孔)受到宽高比的限制。因此,高纵横比结构的微尺度沟槽或孔洞并不容易用标准的DRIE配方获得,而且由于全向限制,微尺度孔洞比沟槽更有问题。在这封信中,我们提出了一种优化的制造高纵横比微尺度孔阵列与改进的横截面蚀刻轮廓。以偏置电压和电感耦合等离子体功率为优化参数,促进高纵横比孔阵列的底蚀。此外,在钝化和脱钝化步骤中,分别考虑了八氟环丁烷(C \(_{4}\) F \(_{8}\))和六氟化硫(SF \(_{6}\))的流量作为降低蚀刻凹损的优化参数。优化后,直径1.3 μm的孔阵列的纵横比达到20,底部的蚀刻面积相对于顶部减少到21%.
Optimization of deep reactive ion etching for microscale silicon hole arrays with high aspect ratio
During deep reactive ion etching (DRIE), microscale etch masks with small opening such as trenches or holes suffer from limited aspect ratio because diffusion of reactive ions and free radicals become progressively difficult as the number of DRIE cycle increases. For this reason, high aspect ratio structures of microscale trenches or holes are not readily available with standard DRIE recipes and microscale holes are more problematic than trenches due to omnidirectional confinement. In this letter, we propose an optimization for fabrication of high aspect ratio microscale hole arrays with an improved cross-sectional etch profile. Bias voltage and inductively coupled plasma power are considered as optimization parameters to promote the bottom etching of the high aspect ratio hole array. In addition, flow rates of octafluorocyclobutane (C\(_{4}\)F\(_{8}\)) and sulfur hexafluoride (SF\(_{6}\)) for passivation and depassivation steps, respectively, are considered as optimization parameters to reduce the etch undercut. As a result of optimization, the aspect ratio of 20 is achieved for 1.3 μm-diameter hole array and etch area reduction at the bottom relative to the top is improved to 21%.