Maria Isabel Arango Torres, Misael Cortés Rodríguez, Esteban Largo Ávila
{"title":"喷雾干燥用雪莲胶状悬浮液的稳定性","authors":"Maria Isabel Arango Torres, Misael Cortés Rodríguez, Esteban Largo Ávila","doi":"10.15446/RFNAM.V72N2.75362","DOIUrl":null,"url":null,"abstract":"Yacon (Smallanthus sonchifolius) is a tuber with a high content of active compounds that offer health benefits, so its productive chain seeks new alternatives to generate yacon products with added value; however, it tends to be a perishable product due to its high aw, chemical composition, and enzymatic activity. The influence of both composition and homogenization in the colloidal stability of yacon suspensions was evaluated for later use in spray drying. Response surface methodology and a central composite design were used, considering three independent variables: homogenization time (TH) (4-6 min), xanthan gum (XG) (0.1-0.2%), and acidity (0.1-0.3%); and the following dependent variables: zeta potential (ζ), color (CIELab), viscosity (μ), stability index by spectral absorption (R), and particle size (D10, D50, and D90). The values of the independent variables that best fit the experimental optimization criteria were: XG=0.16%, acid=0.3%, and TH=4.8 min. The values of the experimental dependent variables and the variables predicted by the quadratic model were ζ=-33.8±4.0 and -37.6 mV, µ=1143.0±93.4 and 1000 cP, R=0.45±0.1 and 0.48, D10=127.8±8.2 and 138.1 µm, D50=251.2±16.3 and 267.7 µm, D90=424.3±28.7 mm and 463.9 µm, L*=41.7±1.4 and 41.8, a*=0.02±0.85 and 1.6, and b*=15.0±1.3 and 14.8, respectively. The colloidal suspension showed adequate physicochemical stability, favored mainly by repulsive forces, homogenization, and rheology of the continuous phase; reaching a content of total solids of 12.5%.","PeriodicalId":37747,"journal":{"name":"Revista Facultad Nacional de Agronomia Medellin","volume":"448 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2019-05-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"3","resultStr":"{\"title\":\"Stability of a colloidal suspension of yacon (Smallanthus sonchifolius) intended for spray drying\",\"authors\":\"Maria Isabel Arango Torres, Misael Cortés Rodríguez, Esteban Largo Ávila\",\"doi\":\"10.15446/RFNAM.V72N2.75362\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Yacon (Smallanthus sonchifolius) is a tuber with a high content of active compounds that offer health benefits, so its productive chain seeks new alternatives to generate yacon products with added value; however, it tends to be a perishable product due to its high aw, chemical composition, and enzymatic activity. The influence of both composition and homogenization in the colloidal stability of yacon suspensions was evaluated for later use in spray drying. Response surface methodology and a central composite design were used, considering three independent variables: homogenization time (TH) (4-6 min), xanthan gum (XG) (0.1-0.2%), and acidity (0.1-0.3%); and the following dependent variables: zeta potential (ζ), color (CIELab), viscosity (μ), stability index by spectral absorption (R), and particle size (D10, D50, and D90). The values of the independent variables that best fit the experimental optimization criteria were: XG=0.16%, acid=0.3%, and TH=4.8 min. The values of the experimental dependent variables and the variables predicted by the quadratic model were ζ=-33.8±4.0 and -37.6 mV, µ=1143.0±93.4 and 1000 cP, R=0.45±0.1 and 0.48, D10=127.8±8.2 and 138.1 µm, D50=251.2±16.3 and 267.7 µm, D90=424.3±28.7 mm and 463.9 µm, L*=41.7±1.4 and 41.8, a*=0.02±0.85 and 1.6, and b*=15.0±1.3 and 14.8, respectively. The colloidal suspension showed adequate physicochemical stability, favored mainly by repulsive forces, homogenization, and rheology of the continuous phase; reaching a content of total solids of 12.5%.\",\"PeriodicalId\":37747,\"journal\":{\"name\":\"Revista Facultad Nacional de Agronomia Medellin\",\"volume\":\"448 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2019-05-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"3\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Revista Facultad Nacional de Agronomia Medellin\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.15446/RFNAM.V72N2.75362\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q3\",\"JCRName\":\"Agricultural and Biological Sciences\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Revista Facultad Nacional de Agronomia Medellin","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.15446/RFNAM.V72N2.75362","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"Agricultural and Biological Sciences","Score":null,"Total":0}
Stability of a colloidal suspension of yacon (Smallanthus sonchifolius) intended for spray drying
Yacon (Smallanthus sonchifolius) is a tuber with a high content of active compounds that offer health benefits, so its productive chain seeks new alternatives to generate yacon products with added value; however, it tends to be a perishable product due to its high aw, chemical composition, and enzymatic activity. The influence of both composition and homogenization in the colloidal stability of yacon suspensions was evaluated for later use in spray drying. Response surface methodology and a central composite design were used, considering three independent variables: homogenization time (TH) (4-6 min), xanthan gum (XG) (0.1-0.2%), and acidity (0.1-0.3%); and the following dependent variables: zeta potential (ζ), color (CIELab), viscosity (μ), stability index by spectral absorption (R), and particle size (D10, D50, and D90). The values of the independent variables that best fit the experimental optimization criteria were: XG=0.16%, acid=0.3%, and TH=4.8 min. The values of the experimental dependent variables and the variables predicted by the quadratic model were ζ=-33.8±4.0 and -37.6 mV, µ=1143.0±93.4 and 1000 cP, R=0.45±0.1 and 0.48, D10=127.8±8.2 and 138.1 µm, D50=251.2±16.3 and 267.7 µm, D90=424.3±28.7 mm and 463.9 µm, L*=41.7±1.4 and 41.8, a*=0.02±0.85 and 1.6, and b*=15.0±1.3 and 14.8, respectively. The colloidal suspension showed adequate physicochemical stability, favored mainly by repulsive forces, homogenization, and rheology of the continuous phase; reaching a content of total solids of 12.5%.
期刊介绍:
La Revista Facultad Nacional de Agronomía Medellín (RFNA), de la Universidad Nacional de Colombia, Sede Medellín, Facultad de Ciencias Agrarias, es una publicación científica editada desde el año 1939, en formato impreso y digital y de acceso abierto desde la web —sin costo para autores y lectores—. Está orientada a investigadores que crean conocimiento disciplinar y multidisciplinar que articula la ciencia y la tecnología para hacer más productivo el campo a nivel empresarial y de economía campesina. La Revista tiene como objetivo divulgar resultados de investigación mediante artículos originales, inéditos y arbitrados (peer review) de carácter científico que respondan a preguntas específicas y que proporcionen sustento y pruebas a una hipótesis, en aspectos relacionados con las Ciencias Agronómicas, Producción animal, Ciencias Forestales, Ingeniería Agrícola, de Alimentos y otras afines que contribuyan a la solución de los limitantes del agro a nivel nacional, regional e internacional. La Revista recibe y publica, sin ningún costo, artículos en idioma inglés de investigación, revisión, reseñas y cartas al editor. Desde el 2017 la periodicidad de publicación es cuatrimestral, se publican tres números al año con circulación nacional e internacional, en los siguientes períodos: Enero - Abril Mayo - Agosto Septiembre - Diciembre This journal does not charge APCs or submission charges.