评价纳米原始AC33对考古陶器的保护和固结过程:与二氧化硅和蒙脱土纳米颗粒的比较研究

Hamdy Mohamed Mohamed, Wael Sabry Mohamed
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引用次数: 3

摘要

目的提供一种有效的纳米复合材料,用于加固和保护变质的考古陶器。设计/方法/方法实验研究中使用了三种纳米复合材料。本研究使用纳米Primal AC33、二氧化硅(SiO2)和蒙脱土(MMT)纳米颗粒来保护和巩固陶器标本。陶器标本在800°C的温度下制作。用刷子涂抹固结材料。利用数字和扫描电子显微镜、静态水接触角、颜色变化、物理性能和抗压强度等多种方法对处理后的陶器样品的性能进行了评估。显微观察表明,Primal AC33/MMT纳米复合材料能够很好地覆盖外表面并与内颗粒结合。对于代码为F的试样,纳米Primal AC33 5%/MMT 3%纳米复合材料处理后,接触角(120°)、密度(1.23 g/cm3)和抗压强度(561 kg/cm2)均有所增加,颜色变化(ΔE = 2.62)、吸水率(4.45%)和孔隙率(5.46%)均有所降低。该结果的新颖性是由于目前研究中使用的纳米Primal AC33 5%/MMT 3%纳米复合材料的特性。原创性/价值本研究描述了本研究中用于评估固结材料的分析方法的重要结果。这一发现为考古陶器的保护提供了有用的信息。研究表明,以Primal AC33 5%/MMT 3%的纳米复合材料效果最好。因此,建议使用这种纳米复合材料来加固考古陶器。因此,目前的工作为保护考古陶器为未来的研究提供了有希望的第一步。
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Evaluating nano Primal AC33 for protection and consolidation processes of archaeological pottery: a comparison study with silica and montmorillonite nanoparticles
Purpose This study aims to offer an effective nanocomposite for potential use to consolidate and protect deteriorated archaeological pottery. Design/methodology/approach Three nanocomposites were used in the experimental study. This study used nano Primal AC33, silicon dioxide (SiO2) and montmorillonite (MMT) nanoparticles to protect and consolidate pottery specimens. Pottery specimens were made at 800°C for this investigation. Consolidation materials were applied with a brush. The properties of the treated pottery specimens were assessed using several methods such as digital and scanning electron microscopes, static water contact angle, color alteration, physical properties and compressive strength. Findings Microscopic examination indicated the ability of the nano Primal AC33/MMT nanocomposites to cover the outer surface well and bind the inner granules. Concerning specimens with code F treated with nano Primal AC33 5%/MMT 3% nanocomposites, it achieved an increase in contact angle (120°), density (1.23 g/cm3) and compressive strength (561 kg/cm2), as well as a decrease in color change (ΔE = 2.62), water absorption (4.45%) and porosity (5.46%). The novelty of the results is due to the characteristics of nano Primal AC33 5%/MMT 3% nanocomposites used in the current study. Originality/value This study describes the significant results of the analytical methods used for evaluating consolidation materials used in this study. The findings offer useful information for the protection of archaeological pottery. The investigation indicated that nano Primal AC33 5%/MMT 3% nanocomposites gave the best results. Therefore, it is recommended to use this nanocomposite to consolidate archaeological pottery. As a result, the current work provides a promising first step in conserving archaeological pottery for future studies.
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