热处理温度对溶胶-凝胶型硅灰石涂层微观结构的影响

Q. Bao, Jia Liu
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引用次数: 0

摘要

采用溶胶-凝胶法制备了不同热处理温度的钛基硅灰石涂层。用XRD分析了试样的显微组织。利用扫描电镜对硅灰石涂层表面形貌进行了观察。结果表明:随着热处理温度的升高,非晶态涂层向结晶涂层转变;当热处理温度高于900℃,PH值为2.5时,溶胶-凝胶法制备的涂层孔隙较多。在这种条件下,涂层不会出现裂纹。
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Effect of Heat Treatment Temperature on Microstructure of Sol-Gel Derived Wollastonite Coating
Wollastonite coatings on titanium alloys substrates were prepared by sol-gel with different heat treatment temperatures. Microstructures of the specimens were analyzed by XRD. SEM was used to observe surface morphologies of wollastonite coatings. The results show that with the heat treatment temperature increasing, the amorphous coating transforms to a crystalline coating. There are many pores in coatings prepared by sol-gel when heat treatment temperature higher than 900°C with the PH value to 2.5. There are no cracks in coating under such conditions.
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