等径角压成形ETP铜的组织与力学性能研究

Ebubekir Atan
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摘要

剧烈塑性变形(SPD)是指材料在高压下发生的塑性变形,用于改善材料的力学性能和结构性能。等通道角挤压(ECAP)是一种通过两个直径相同的角相交通道对样品施加高压以产生亚微米或纳米级颗粒的材料微观结构的方法。近年来,对纳米颗粒金属材料制备的研究日益增多。本研究的目的是研究高压下材料的微观结构和力学性能的逐渐变化,并确定ECAP对这些性能改善的影响。这个过程直接关系到材料的内部结构和纹理。该方法旨在获得更耐用的材料结构。本研究选择了电工常用的铜材料之一——电解韧性铜材料(ETP)。12毫米直径和35毫米长的ETP铜样品,没有经过任何热处理,在2毫米/秒的冲压速度,200°C的模具温度和Bc ECAP路线上,使用120吨容量的液压机,一个精密加工的模具,有120°(Φ=120°,ψ=20°)通道角。研究了应用ECAP后样品的晶体结构、微观结构和力学性能的变化。结果表明,经4道次ECAP处理后,合金组织晶粒细化,力学性能得到改善。
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Investigation of Microstructure and Mechanical Properties of ETP Copper Deformed by Equal Channel Angular Pressing (ECAP)
Severe plastic deformation (SPD), the plastic deformation of materials under high pressure, is used to improve the mechanical and structural properties of materials. Equal Channel Angular Pressing (ECAP) is one of these methods used to produce materials microstructure with submicron or nano-sized grains by applying high pressure to the sample passing through two angular intersecting channels with the same diameters. In recent years, studies on the production of nano-grained metallic materials have increased. The aim of this study is to examine the gradual change of the microstructure and mechanical properties of the material under high pressure and to determine the effect of ECAP on the improvement of these properties. This process is directly related to the internal structure and texture of the material. With the applied method, it is aimed to obtain a more durable material structure. Electrolytic Tough Pitch (ETP) copper material, which is one of the copper types commonly used in electrical applications, was chosen in the study. 12 mm diameter and 35 mm long ETP copper samples, which were not subjected to any heat treatment, processed on 2 mm/s pressing speed, 200°C mold temperature and Bc ECAP route using a 120 ton capacity hydraulic press, a precision machined mold which has 120° (Φ=120°, ψ=20°) channel angle. The changes in the crystal structure, microstructure and mechanical properties of the ECAP applied samples were investigated. According to the data obtained, it was observed that the 4 passes of ECAP application resulted in having finer grains in microstructure and improvement in mechanical properties.
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