用特高压STM观察电子发射尖端的结构

Kazuki Noda, Miyuki. Tanaka, N. Watanabe, T. Kubo, Tetsuo Shimizu
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摘要

电子发射尖端广泛应用于微细加工、电子显微镜、表面科学等诸多研究领域。电子发射体主要有三种类型:热离子型、场发射型和肖特基型。ZrO2包覆的钨< 100 >单晶由于具有高稳定性和大发射电流,被广泛用作电子显微镜的肖特基电子发射器。为了开发一种评价电子发射体的新技术,我们认为用扫描探针显微镜观察电子发射尖端的表面形貌结构是可能的,并成功地观察了空气中电子发射尖端的纳米结构。在这项研究中,我们尝试使用超高真空扫描隧道显微镜(UHVSTM)来观察尖端的纳米结构,因为电子发射器通常在特高压条件下使用。利用特高压STM,获得了与扫描电镜图像相关的高分辨率STM图像。这表明,特高压STM可能是一个可信的工具,电子尖端的表征。
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Structural Observation of Electron Emitting Tip Using UHV STM
Electron emitting tip is widely used in many research ˆelds such as microfabrication, electron microscopy, surface science and so on. There are mainly three types of electron emitter as thermionic, ˆeld-emission and Schottky electron emitter. Because of the high stability with large emission current, tungsten〈100〉single crystal coated with ZrO2 is widely used as Schottky electron emitter of an electron microscope. In order to develop a new technique for evaluating electron emitter, we thought that it was possible to observe the surface topographic structures of the electron emitting tip with a scanning probe microscope and succeeded in observing the nanostructure of the electron emitting tip in air. In this study, we have tried to observe tip nanostructure using ultra high vacuum scanning tunneling microscope (UHVSTM), because electron emitter is generally used under UHV condition. Using UHVSTM, high resolution STM images which are related to scanning electron microscope images were acquired. This indicated that UHVSTM could be a plausible tool for electron tip characterization.
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