气相色谱-质谱联用及傅里叶变换红外光谱分析大戟的生物活性成分

Azhar Abduameer Sosa, Suhaila Husaein Bagi, I. Hameed
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引用次数: 56

摘要

研究了大戟种子甲醇提取物的植物化学成分。气相色谱分析-质谱法(gc - ms)分析的大肠lathyrus显示碳酸的存在,(乙)(1、2、4-triazol-1-ylmethyl)二酯,1 h-pyrrole, 2, 5-dihydro-1-nitroso,己醛二甲缩醛,硝酸异山梨酯,DL-Arabinose,环丙烷,1-fluoro-1——(2-bromoethenyl) 2, 2, 3, 3-tetramethyl,α-D-Glucopyranoside, O -α-D-glucopyranosyl - (1. fwdarw.3) -s-d-fruc Desulphosinigrin,葡萄糖,6 -α-D-galactopyranosyl,辛酸,香豆酮,2,3-dihydro, 6-Acetyl-s-d-mannose,草蒿脑、环氧Ascaridole 3-Allyl-6-methoxyphenol 4-Amino-1 5, pentandioic酸,l-Gala-l-ido-octonic内酯,y-Sitosterol,十四酸、l -(+)抗坏血酸2,6-dihexadecanoate, Estra 1, 3, 5 (10) -trien-17s-ol,丙酸、2 - (3-acetoxy-4 4 14-trimethylandrost-8-en-17-yl) Cis-13-Eicosenoic酸、花生酸、3-Pyrinecarboxylic酸,2、7,10-tris (acetyloxy) 1, 1, 2, 3, 4, 6, 7, 10,油酸,eicosyl酯,丁酸,4-chloro - 1, 1, 1, 4, 4, 5, 7, 7 b, 8日9-decahydro-4a,异胆酸乙酯,异胆酸乙酯,齐墩-12-烯-3,15,16,21,22,28-己醇,(3s,15α,16α,21 α, 22α)-和2,4,6-十三烯酸,1,2,5,5,5a,6,9,10,10a-八氢-5,5 -二羟基。傅里叶变换红外光谱(FTIR)分析证实了石竹种子中存在烯烃、脂肪族氟化合物、醇类、醚类、羧酸类、酯类、硝基化合物、烷烃、氢键醇和酚类化合物。关键词:气相色谱-质谱(GC/MS),生物活性化合物,傅里叶变换红外光谱(FT-IR),大戟
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Analysis of bioactive chemical compounds of Euphorbia lathyrus using gas chromatography-mass spectrometry and Fourier-transform infrared spectroscopy
The aim of this study was determination the phytochemical composition of methanolic seeds extract of Euphorbia lathyrus. Gas chromatography-mass spectrometry (GC-MS) analysis of E. lathyrus revealed the existence of the Carbonic acid, (ethyl)(1,2,4-triazol-1-ylmethyl) diester, 1H-Pyrrole,2,5-dihydro-1-nitroso, Hexanal dimethyl acetal,  Isosorbide dinitrate, DL-Arabinose, Cyclopropane,1-fluoro-1-(2-bromoethenyl)-2,2,3,3-tetramethyl, α-D-Glucopyranoside, O-α-D-glucopyranosyl-(1.fwdarw.3)-s-d-fruc, Desulphosinigrin, D-Glucose, 6-O-α-D-galactopyranosyl, Octanoic acid, Benzofuran,2,3-dihydro, 6-Acetyl-s-d-mannose, Estragole, Ascaridole epoxide, 3-Allyl-6-methoxyphenol, 4-Amino-1,5,pentandioic acid, l-Gala-l-ido-octonic lactone, y-Sitosterol, Tetradecanoic acid, l-(+)-Ascorbic acid 2,6-dihexadecanoate, Estra -1,3,5(10)-trien-17s-ol, Propanoic acid,2-(3-acetoxy-4,4,14-trimethylandrost-8-en-17-yl), Cis-13-Eicosenoic acid, Eicosanoic acid, 3-Pyrinecarboxylic acid, 2,7,10-tris(acetyloxy)-1,1a,2,3,4,6,7,10, Oleic acid, eicosyl ester, Butanoic acid, 4-chloro-,1,1a,1b,4,4a,5,7a,7b,8,9-decahydro-4a, Ethyl iso–allocholate, Ethyl iso –allocholate, Olean-12-ene-3,15,16,21,22,28-hexol, (3s,15α,16α,21s,22α)- and 2,4,6-Decatrienoic  acid,1a,2,5,5a,6,9,10,10a-octahydro-5,5a-dihy. The Fourier-transform infrared spectroscopy (FTIR) analysis of E. lathyrus seeds proved the presence of alkenes, aliphatic fluoro compounds, alcohols, ethers, carboxlic acids, esters, nitro compounds, alkanes, hydrogen bonded alcohols, and phenols.   Key words: Gas chromatography-mass spectrometry (GC/MS), bioactive compounds, Fourier-transform infrared spectroscopy (FT-IR), Euphorbia lathyrus.
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