以天然石英砂为原料合成纳米有序介孔二氧化硅

T. F. Kouznetsova, V. Agabekov, A. Ivanets, E. V. Karpinchik, J. Sauka
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引用次数: 0

摘要

从天然石英砂中获得了具有有序纳米结构的介孔分子筛,具有圆柱形孔的立方填充和三维多孔结构。通过x射线衍射、扫描电镜和低温氮吸附-脱附实验表明,所制得的二氧化硅材料热稳定,无定形,由亚微米颗粒组成,比表面积高达1396 m2/g,孔体积为0.780 cm3/g,平均直径为2.2 nm,介孔尺寸分布窄。
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Synthesis of mesoporous silica with ordered nanostructural morphology from natural quartz sand
Silica with ordered nanostructured morphology characteristic of mesoporous molecular sieves with cubic packing of cylindrical pores and a three-dimensional porous structure is obtained from natural quartz sand. It was shown by X-ray diffraction, scanning electron microscopy, and low-temperature nitrogen adsorption-desorption that the obtained silica material is thermally stable, amorphous, consists of submicron grains, has a high specific surface area of 1396 m2/g, a pore volume of 0.780 cm3/g and an average diameter of 2.2 nm with a narrow size distribution of mesopores.
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