Cu-TSV单轴微拉伸试验独立试样的设计与制作

Junyi Li, Hong Wang, Huiying Wang, Z. Zhang, P. Cheng, G. Ding
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引用次数: 1

摘要

本文提出了一种新型的用于单轴微拉伸试验的Cu-TSV微尺度独立试样。设计了变形缓冲网状支撑架,有效降低了Cu-TSV薄膜在夹紧过程中的变形。通过在表面处理过的钛种层上制备Cu-TSV薄膜,使电沉积过程中产生的应力最小化。与传统的Cr/Cu种层工艺相比,钛种层工艺避免了碱腐蚀,简化了制作工艺。有限元模拟和实验结果均表明了该设计的优越性。经优化的工艺制备的试样与微拉伸系统配合良好。微拉伸系统测得Cu-TSV薄膜的杨氏模量和极限拉伸强度分别为25.4 ~ 32.9GPa和574 ~ 764MPa。
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Design and fabrication of Cu-TSV free-standing specimen for uniaxial micro-tensile test
A novel test sample with a micro scale free-standing specimen of Cu-TSV used for uniaxial micro-tensile test is presented in this paper. Design of a deformation-buffer reticular supporting frame of the test sample effectively reduces the deformation of Cu-TSV thin film during clamping operation. The stress resulting from electrodepositon process is minimized by fabricating Cu-TSV thin film on surface-treated titanium seed layer. The process of titanium seed layer avoids alkali corrosion and simplifies fabrication procedure compared with that of the traditional Cr/Cu seed layer. Both finite-element method (FEM) simulation and experimental results indicates the advantages of this new design. The test sample fabricated by the optimized process well coordinates with our micro-tensile system. The Young's modulus and the ultimate tensile strength of tested Cu-TSV thin film measured by our micro-tensile system are 25.4∼32.9GPa and 574∼764MPa, respectively.
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