无溶剂条件下h -沸石a催化合成14-芳基- 14h -二苯并[a,j]杂蒽衍生物

S. Bhat, Rawoof Ahmad Naikoo, M. A. Mir, R. Bhat, M. Malla, R. Tomar
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引用次数: 6

摘要

h -沸石A是一种高效、优良、可重复使用的催化剂,用于无溶剂条件下β-萘酚与各种芳醛衍生物一锅合成14-芳基- 14h -二苯并[A,j]杂蒽衍生物。采用XRD、SEM和FT-IR对合成的h型A沸石进行了表征。通过FT-IR和1H-NMR对合成产物进行了表征。这些反应的特点是工序简单、反应时间短、收率高、催化剂可重复使用。
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Synthesis of 14-Aryl-14H-dibenzo[a,j]xanthene Derivatives Using H-Zeolite A as an Efficient and Reusable Catalyst under Solvent-Free Condition
H-Zeolite A is an efficient, excellent, and reusable catalyst for the synthesis of 14-aryl-14H-dibenzo[a,j]xanthene derivatives by one-pot synthesis of β-naphthol with various aromatic aldehyde derivatives under solvent-free condition. The synthesized zeolite H-Zeolite A was characterized by XRD, SEM, and FT-IR. The synthesized products were characterized by FT-IR and 1H-NMR spectra. Simple workup procedure, short reaction time, high yield, and reusability of the catalyst are the characteristic features of these reactions.
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