芙蓉花绿色合成氧化铁纳米颗粒及其抗菌活性研究

IF 3.9 Q2 NANOSCIENCE & NANOTECHNOLOGY Journal of Nanotechnology Pub Date : 2022-03-10 DOI:10.1155/2022/5474645
F. Buarki, H. AbuHassan, F. Al Hannan, F. Henari
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引用次数: 26

摘要

以芙蓉花(常用名称,月季)提取物为还原剂和稳定剂,采用非常规环保技术合成了氧化铁纳米颗粒(α- Fe2O3)。采用微波法制备了氧化铁纳米颗粒。采用不同体积比的四水氯化铁与萃取物,在微波炉中加热不同时间,以优化氧化铁纳米颗粒的产量。采用紫外可见光谱(UV-Vis)、傅里叶变换红外光谱(FTIR)、透射电子显微镜(TEM)和x射线衍射(XRD)对合成的氧化铁纳米颗粒进行了表征。x射线衍射证实了α- Fe2O3纳米颗粒(赤铁矿)的形成。氧化铁纳米颗粒的平均尺寸为51 nm。研究了合成的铁纳米颗粒对金黄色葡萄球菌、铜绿假单胞菌、肺炎克雷伯菌和大肠杆菌等细菌的抑菌活性。结果表明,所合成的铁纳米颗粒对所研究的细菌均有一定的居住作用。
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Green Synthesis of Iron Oxide Nanoparticles Using Hibiscus rosa sinensis Flowers and Their Antibacterial Activity
Iron oxide nanoparticles (α- Fe2O3) were synthesized using an unconventional, eco-friendly technique utilizing a Hibiscus rosa sinensis flower (common name, China rose) extract as a reducer and stabilizer agent. The microwave method was successfully used for the synthesis of iron oxide nanoparticles. Various volume ratios of iron chloride tetrahydrate to the extract were taken and heated by the microwave oven for different periods to optimize iron oxide nanoparticle production. The synthesized iron oxide nanoparticles were characterized using the ultraviolet-visible spectrometer (UV-Vis), Fourier transform infrared spectroscopy (FTIR), transmission electron microscopy (TEM), and X-ray diffraction (XRD). X-ray diffraction confirmed the formation of α- Fe2O3 nanoparticles (hematite). The average size of iron oxide nanoparticles was found to be 51 nm. The antibacterial activity of the synthesized iron nanoparticles was investigated against different bacteria such as Staphylococcus aureus, Pseudomonas aeruginosa, Klebsiella pneumonia, and Escherichia coli. The results showed that the synthesized iron nanoparticles exhibited an inhabitation effect on all studied bacteria.
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来源期刊
Journal of Nanotechnology
Journal of Nanotechnology NANOSCIENCE & NANOTECHNOLOGY-
CiteScore
5.50
自引率
2.40%
发文量
25
审稿时长
13 weeks
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