溶胶-凝胶法交联对锡纳邦山火山灰与虾壳复合材料性能的影响

Lisnawaty Simatupang, M. Situmorang, R. Siburian, B. Wirjosentono
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引用次数: 0

摘要

采用溶胶-凝胶法研究了戊二醛交联对锡纳邦火山灰na2sio3前驱体与虾壳壳聚糖合成二氧化硅壳聚糖复合材料的影响。以戊二醛为交联剂,不含戊二醛,将20ml na2sio3前驱体与(2%:3%)(w/v)壳聚糖混合,合成了二氧化硅-壳聚糖复合材料。溶胶-凝胶修饰是一种更简单、更快速的修饰方法,同时也是一种可调动配体的结合反应。用戊二醛标记(Si-g-ChC)和无戊二醛标记(SiChC)制备了二氧化硅壳聚糖复合材料。用FTIR和XRD分析了复合材料(Si-g-ChC)和(SiChC)的性能。
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Effect Croslinking on Characteristics of Silica Chitosan Composite from Vulcanic Ash of Sinabung Mount and Shrimp Husk by Sol Gel Method
: This research was carried out to determine the effect of glutaraldehyd croslinking on the synthesis of silica chitosan composites from the Na 2 SiO 3 precursor of volcanic ash of Sinabung and chitosan from shrimp husk by sol gel method. The synthesis of the silica-chitosan composite by mixing the 20 mL Na 2 SiO 3 precursors with (2% : 3%) (w/v) chitosan in the aid of glutaraldehyde as crosslinking agent and without glutaraldehyde. Modifications with sol gel is done because it is more simple and rapid progress as well as the binding reaction of the ligands mobilized. Prepared Silica Chitosan Composit using glutaraldehyd labeled (Si-g-ChC) and Silica Chitosan Composit without glutaraldehyd labeled (SiChC) . The characteristic of the composit material (Si-g-ChC) and (SiChC) used by FTIR and XRD.
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