烧结对CaTiO3纳米陶瓷时域响应的影响

Subhanarayan Sahoo
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引用次数: 0

摘要

高能球磨(HEBM)用于合成纳米晶钛酸钙CaTiO3 (CT)陶瓷。采用x射线衍射(XRD)、阻抗和时域分析进行表征。从奈奎斯特图的复杂阻抗谱中观察到一个半圆弧的出现对晶粒传导的影响。计算了各种时间响应参数。在1000℃、1100℃和1200℃下烧结成圆盘状的绿色球团,研究烧结对时间响应的影响。利用部分分式和拉普拉斯逆变换方法对各样本的cole-cole图得到的等效电路参数进行MATLAB编程得到时域响应。该研究证明了纳米CaTiO3作为电气和电子设备应用中更快敏感材料的潜力。
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Effect of Sintering on Time Domain Response of CaTiO3 Nano Ceramics
High-energy ball milling(HEBM) used for synthesize nano crystalline Calcium Titanate, CaTiO3 (CT) ceramic. X-ray diffraction(XRD), impedance and time domain analysis applied for characterization. Effect of grain conduction observed from complex impedance spectrum in the Nyquist plot by the appearance of one semi-circular arc. Various time response parameters have been calculated. Green pellets in disk shaped sintered at 1000°C, 1100°C and 1200°C to study the effect of sintering on time response. Time domain response obtained by MATLAB programming of equivalent circuit parameters got from cole-cole plot of respective samples using partial fraction and inverse Laplace transform method. Potential of nano CaTiO3 as faster sensitive material for electrical and electronic device applications proven by the study.
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