埃及油页岩填料在锂基润滑脂生产中的新应用

M. Al-Wakeel, R. El-Adly
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引用次数: 11

摘要

本文报道了以油页岩为填料,以大豆皂基和芳香烃提取物为基础的6种油脂配方的制备和表征。对Quseir-Safaga地区的油页岩进行了详细的岩石学、粒度分布、矿物学和化学研究。用有机溶剂对提取的总烃含量进行凝胶渗透色谱(GPC)的分子量分析。测定了芳香提取物的理化性质。优化了混合后的加工条件,以生产合适的锂皂结构,以及填料的分散性。这项工作还包括研究不同等级的芳香提取物和不同百分比的油页岩的竞争效率,以及评估它们对配方润滑脂性能的影响。根据国家润滑脂协会(NLGI)和埃及标准(ES)对制备的润滑脂进行评估。综上所述,上述成分可用于锂脂的制备。
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A Novel Application of Egyptian Oil Shale as a Filler in the Production of Lithium Lubricating Grease
This article reports on the preparation and characterization of six formulations of grease based on soybean soapstock and aromatic extracts using oil shale as a filler. The oil shale that occurs within the Quseir–Safaga district is subjected to a detailed petrography, size distribution, mineralogy, and chemical studies. The total extracted hydrocarbon content, using an organic solvent, is analyzed for molecular weight by gel permeation chromatography (GPC). The physicochemical properties of the aromatic extracts are determined. The processing conditions following the blending are optimized to produce the appropriate lithium soap structure, as well as dispersion of the filler. The work also includes a study of the competitive effectiveness of different grades of aromatic extracts and also various percentages of oil shale, along with an evaluation of their effects on the properties of formulated lubricating greases. The prepared greases are assessed in accordance with National Lubricating Grease Institute (NLGI) and Egyptian Standard (ES). It is concluded that the above-mentioned ingredients can be used for the preparation of lithium greases.
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