表面磨削金属粉末:激光烧结的适用性及性能评价

Harish Singh Dhami, Pritish Panda, Puli Saikiran, K. Viswanathan
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摘要

作为增材制造(AM)应用的原料的商业金属粉末主要通过气体或水雾化技术生产。这些都是高度资本密集型和不灵活的,使得所得粉末比相应的铸锭贵3-10倍。最近,我们已经证明了一种潜在的替代路线,使金属粉末-使用表面磨削。所得到的粉末已经显示出在金属定向能沉积(DED)工艺中用作库存的希望。这项工作探讨了这些替代生产粉末在激光烧结和相关应用中的适用性。在5-100微米范围内的球形金属粉末颗粒(AISI 52100, SS 304)首次使用表面磨削生产。这些粉末经过后处理并分离成单分散批次和多分散批次,分别代表优质-低收率和低品质-高收率的原料。利用光斑直径为50微米的高功率光纤激光源,在氮气保护气体下对这两种原料粉进行烧结,并使用一系列非原位分析技术对其性能进行了评估。后者包括金相、SEM/EDS和XRD分析,并用于评估两种情况下的烧结质量,包括熔池和热影响区表征。基于这些结果,我们提出了单分散和多分散金属粉末的使用建议,并展示了使用研磨作为激光烧结应用中金属粉末生产的替代技术的潜在效用。
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Metal Powders via Surface Grinding: Applicability and Performance Evaluation for Laser Sintering
Commercial metal powders used as feedstock for additive manufacturing (AM) applications are primarily produced via gas or water atomization techniques. These are highly capital-intensive and inflexible, making the resulting powders as much as 3–10 times more expensive than corresponding cast ingots. Recently, we have demonstrated a potential alternative route for making metal powders — using surface grinding. The resulting powders have shown promise for use as stock in metal directed energy deposition (DED) processes. This work explores the applicability of these alternatively produced powders for laser sintering and related applications. Spherical metal powder particles (AISI 52100, SS 304) in the range of 5–100 microns were first produced using surface grinding. These powders were post-processed and segregated into monodisperse and polydisperse batches, representing high quality-low yield and low-quality-high yield stock, respectively. A high-power fiber laser source of 50 microns spot diameter was used to sinter these two stock powders, with nitrogen as a shielding gas, and their performance was evaluated using a range of ex situ analysis techniques. The latter included metallography, SEM/EDS and XRD analysis and was used to evaluate sintering quality in both cases, including melt pool and heat-affected zone characterization. Based on these results, we present recommendations for the use of mono- and polydisperse metallic powders and demonstrate the potential utility of using grinding as an alternative technique for the production of metal powders for laser sintering applications.
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