化学-机械法修饰纳米红树淀粉及其制备水凝胶的应用

G. Saragih, Tamrin, Marpongahtun, D. Nasution
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引用次数: 1

摘要

红树林是一种保护陆地免受海浪侵袭的植物。红树林是一种尚未被开发的淀粉来源。为了扩大应用,需要对淀粉进行改性。天然淀粉是用湿法提取的。采用化学-机械方法合成天然淀粉为纳米淀粉。改性红树果淀粉可用作制备水凝胶的基质。表征淀粉和淀粉纳米颗粒包括代理分析,官能团使用傅里叶变换红外光谱(FTIR)。测试PSA(粒度分析仪),找出粒度。用x射线衍射(XRD)测试淀粉纳米颗粒的结晶度。利用扫描电子显微镜(SEM)对纳米颗粒进行形貌分析。热测试使用差示扫描量热计(DSC)。结果表明,红树淀粉的产率为29.60%,红树淀粉纳米颗粒的粒径为38.79 nm。在1050 ~ 1300 cm的吸收区(此振动表示氢与C-O键的拉伸区振动)。红外光谱分析结果表明,红树林淀粉提供了描述淀粉结构的光谱。
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Modification and Characterization Starch Nanoparticles of Mangrove Fruit using Chemical-mechanical Method and Application as Basic Materials Making Hydrogel
: Mangroves are plants that function as protectors of the land from ocean waves. Mangroves are a source of starch that has not been explored. To expand the application, the starch needs to be modified. Natural starch is made using wet extraction. Natural starch is synthesized into nanoparticle starch by chemical-mechanical methods. Modified Mangrove Fruit Starch can be used as a base for making hydrogels. Characterization of starch and starch nanoparticles includes proxy analysis, functional groups using the Fourier Transform Infrared Spectroscopy (FTIR). Test the PSA (Partiicle size analyzer) to find out the particle size. Crystallinity test of starch nanoparticles using X-Ray Diffraction (XRD). The morphological analysis of nanoparticles was carried out using the Scanning Electron Microscopy (SEM) instrument. Thermal test using Differential scanning calorimeter (DSC). The results showed that mangrove starch had a yield of 29.60% and particle size of mangrove nanoparticles of 38.79 nm. cyclic or aromatic ring and in the absorption area of 1050 - 1300 cm -1 This vibration shows the vibration of the stretching region of hydrogen with the C-O bond). The results of FTIR spectroscopic analysis showed that the mangrove starch provides a spectrum that describes the structure of starch.
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