椰壳炭合成石墨烯

M. Supeno, R. Siburian, Desi Natalia
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引用次数: 1

摘要

混合椰壳炭为sp3,与活性炭混合,加热至600(cid:31) 1小时后产生sp2,表现出石墨烯的表征。本研究制备石墨烯的工艺是将椰子壳在阳光下晒干,然后水解成木炭,再与活性炭作为还原剂在600℃下混合1小时生成石墨烯。用XRD、SEM-EDX、XRF和BET对所得石墨烯进行了表征。XRD分析结果表明,所得峰不尖锐,在24°和44°处衍射峰略有加宽。在4000倍放大下的SEM-EDX分析结果显示,石墨烯的表面尺寸和结构形状更小、更薄,石墨烯结构中的堆积也减少了。XRF分析结果表明,仍有有机杂质存在。石墨烯的BET分析结果表明,石墨烯的表面积为82.873 m2 / g,孔隙体积为0.116 cc / g。
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The Synthesis of Graphene from Coconut Shell Charcoal
: The hybrid coconut shell charcoal is sp 3 , after being mixed with activated carbon and heated to 600(cid:31) for 1 hour it produces sp 2 which shows the characterization of graphene. The process of making graphene in this study, namely coconut shell dried under sunlight then hydrolyzed into charcoal then mixed with activated carbon as a reducing agent at 600°C for 1 hour to produce graphene. The resulting graphene is characterized by XRD, SEM-EDX, XRF and BET. The results of the XRD analysis showed that the resulting peaks were not sharp and slightly broadened the diffraction peak at 24° and 44°. The results of SEM-EDX analysis at 4000x magnification showed smaller, thinner surface sizes and structural shapes and reduced buildup in the graphene structure. XRF analysis results show that there are still organic impurities. The results of graphene analysis with BET show the surface area of graphene 82.873 m 2 / g with a pore volume of 0.116 cc / g.
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