工作频率在400兆赫和1千兆赫之间的超高频EPR光谱仪

IF 0.9 4区 医学 Q4 CHEMISTRY, PHYSICAL Concepts in Magnetic Resonance Part B-Magnetic Resonance Engineering Pub Date : 2016-10-31 DOI:10.1002/cmr.b.21328
Richard W. Quine, George A. Rinard, Yilin Shi, Laura Buchanan, Joshua R. Biller, Sandra S. Eaton, Gareth R. Eaton
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引用次数: 7

摘要

设计并构建了一台光谱仪,用于测量T1、T2、自旋回波信噪比和谐振器质量因子Q,测量范围在400 ~ 1000 MHz之间。脉冲模式在250兆赫产生,并与第二源的输出混合,以执行激励和检测。设计了一种跨环谐振器,可以在同一谐振器中测量相同的样品在整个频率范围内。建立了一个具有大实验体积的空芯、四圈、水冷式电磁铁。
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UHF EPR spectrometer operating at frequencies between 400 MHz and 1 GHz

A spectrometer was designed and constructed to facilitate measurements of T1, T2, spin echo signal-to-noise, and resonator quality factor, Q, between about 400 and 1000 MHz. Pulse patterns are generated at 250 MHz and mixed with the output from a second source to perform excitation and detection. A cross-loop resonator was constructed in which the same sample could be measured in the same resonator over the full range of frequencies. An air-core, four-coil, water-cooled electromagnet with a large experimental volume was built.

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来源期刊
CiteScore
2.60
自引率
0.00%
发文量
3
审稿时长
>12 weeks
期刊介绍: Concepts in Magnetic Resonance Part B brings together engineers and physicists involved in the design and development of hardware and software employed in magnetic resonance techniques. The journal welcomes contributions predominantly from the fields of magnetic resonance imaging (MRI), nuclear magnetic resonance (NMR), and electron paramagnetic resonance (EPR), but also encourages submissions relating to less common magnetic resonance imaging and analytical methods. Contributors come from both academia and industry, to report the latest advancements in the development of instrumentation and computer programming to underpin medical, non-medical, and analytical magnetic resonance techniques.
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