Huixiao Duo , Jiayuan Yue , Xiaodan Zhang , Siqi Li , Yujian Yin , Liyun Wang , Jiejia Li , Weiwei Rong , Andong Wang , Yuan Zhang , Qing Zhu
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Magnetic solid phase extraction based on metal organic framework for pharmaceutical analysis from food, environmental and biological media
Magnetic solid-phase extraction (MSPE) is gaining increasing attention in the study of extracting pharmaceutical molecules from complex matrices, which can be attributed to the emergence of adsorbents such as metal–organic frameworks (MOFs). Magnetic MOFs (MMOFs) show great potential in adsorption and separation of pharmaceuticals in complex substrates due to their large surface area, uniformly adjustable pore size and easy recovery. This paper reviews the recent progress of MMOFs in extraction and detection of various pharmaceutical from food, environment and biological samples. The preparation methods of different types of Fe3O4-based magnetic MOFs and MOFs-derived magnetic carbon adsorbents are also briefly introduced. Finally, the challenges and research directions of MMOFs in the field of pharmaceutical analysis are discussed and elaborated. This paper aims to provide theoretical basis for the development and application of emerging MMOFs extractants, and expand new directions for the extraction and analysis of pharmaceuticals.
期刊介绍：
The Microchemical Journal is a peer reviewed journal devoted to all aspects and phases of analytical chemistry and chemical analysis. The Microchemical Journal publishes articles which are at the forefront of modern analytical chemistry and cover innovations in the techniques to the finest possible limits. This includes fundamental aspects, instrumentation, new developments, innovative and novel methods and applications including environmental and clinical field.
Traditional classical analytical methods such as spectrophotometry and titrimetry as well as established instrumentation methods such as flame and graphite furnace atomic absorption spectrometry, gas chromatography, and modified glassy or carbon electrode electrochemical methods will be considered, provided they show significant improvements and novelty compared to the established methods.
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