Impact of deposition parameters on the characterizations of highly orientated aluminum nitride for film bulk acoustic wave resonator device

J. Ning, R.K. Sharma, Feng Hanhua, Wang Zhe, S. Xu
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Abstract

AlN thin films were grown on Si(100) and Al/Si(100) substrates by pulsed dc sputtering system using 99.999% purity aluminum as target, and Ar+N/sub 2/ gas mixture as precursor. The impact of deposition parameters, including dc power, deposition pressure and substrate temperature, on material properties has been investigated. A good correlation between film crystallinity and dc power, as well as gas pressure, was addressed by X-ray diffraction, and verified by scanning electron microscope (SEM) and ellipsometry. It is found that highly c-axis oriented h-AlN can be obtained at low gas pressure and low deposition rate. For AlN on Al/Si(100) substrate, micro-crack was observed, which was assigned to the large thermal stress between AlN film and Al layer. Crack-free surface has been achieved by reducing the deposition temperature. The deposition mechanism of AlN deposition is discussed. This work provides a material foundation for film bulk wave resonator (FBAR) devices fabrication.
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沉积参数对膜体声波谐振器高取向氮化铝表征的影响
以纯度为99.999%的铝为靶材,Ar+N/sub - 2/气体混合物为前驱体,采用脉冲直流溅射系统在Si(100)和Al/Si(100)衬底上生长了AlN薄膜。研究了沉积参数(包括直流功率、沉积压力和衬底温度)对材料性能的影响。通过x射线衍射分析了薄膜结晶度与直流功率和气体压力之间的良好相关性,并通过扫描电镜和椭偏仪进行了验证。研究发现,在低气压和低沉积速率条件下,可获得高度c轴取向的h-AlN。对于Al/Si(100)衬底上的AlN,观察到微裂纹,这是由于AlN膜与Al层之间存在较大的热应力。通过降低沉积温度,实现了无裂纹表面。讨论了AlN沉积机理。本研究为薄膜体波谐振器(FBAR)器件的制备提供了物质基础。
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