Microwave impedance microscopy of high specific surface area carbon

Timothy S. Jones, C. R. Perez, J. Santiago-Avilés, Keith Jones
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Abstract

Microwave impedance microscopy (MIM) is a novel scanning probe technique used to measure local electrical impedance under an AFM tip operating at some fixed electrical resonant frequency. Each point in the surface scan records sample elevation and power return loss, thus generating a topographical image with an overlaid impedance map. Various high specific surface area (SSA) carbon materials, recently demonstrated to have excellent performance as electrochemical capacitor electrodes, were investigated via MIM. Results of MIM studies on these materials may be used to provide additional understanding of transport properties and complement conventional methods of surface area measurement.
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高比表面积碳的微波阻抗显微镜
微波阻抗显微镜(MIM)是一种新型扫描探针技术,用于测量在固定电谐振频率下工作的原子力显微镜针尖下的局部电阻抗。在表面扫描的每个点记录样品的高程和功率返回损耗,从而产生地形图像与叠加阻抗图。利用MIM技术研究了各种高比表面积(SSA)碳材料作为电化学电容器电极的优异性能。对这些材料的MIM研究结果可用于提供对输运性质的额外理解,并补充传统的表面积测量方法。
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