Penentuan Kondisi Optimum Waktu Aging dan Temperatur Pengeringan Pada Sintesis Silika Xerogel dengan Bahan Dasar Natrium Silikat dari Silika Alam

Elvina Yulistia Erwan, Budhi Oktavia
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Abstract

Abstract — Silica is one kind of porous material that is suited to adsorben. In the synthesis process, silica gel can be produced using a sol-gel method based on the sodium silicate (Na2SiO3), which is prepared by an acid. The project of this research is to establish optimum conditions in aging time and gel-drying temperatures to produce a broad surface and pore size for silica xerogel. Based on the iod's absorption of variations in aging time (14, 16, 18, 20 and 24 hours) and drying temperatures (60, 70, 80, 90 and 100°C) give the most absorption to optimum conditions of aging time at 18 hours and drying temperatures of 70°C. The presence of XRD pattern leads to amorphous nature structures that dilate at one peak in 2θ = 22.545°, which indicates synthesis of silica xerogel with a basic sodium silicate obtained from natural silica was successfully made and highly pure. Keywords — Silica, Sodium Silicate, Silica xerogel 
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用天然二氧化硅钠合成合成物的最佳时间加热和温度
摘要:二氧化硅是一种适合于吸附的多孔材料。在合成过程中,以酸法制备的硅酸钠(Na2SiO3)为原料,采用溶胶-凝胶法制备硅胶。本研究的目的是确定老化时间和凝胶干燥温度的最佳条件,以获得宽表面和孔径的二氧化硅干凝胶。通过对不同陈化时间(14、16、18、20和24小时)和干燥温度(60、70、80、90和100℃)变化的吸收,得出18小时陈化时间和70℃干燥温度的最佳条件吸收最多。XRD图谱的存在导致了在2θ = 22.545°处有一个峰膨胀的无定形结构,这表明以天然二氧化硅为原料制备的碱式水玻璃成功合成了二氧化硅干凝胶,纯度高。关键词:二氧化硅,硅酸钠,二氧化硅干凝胶
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