Structural and surface studies of the cdse thin films deposited by close space sublimation method

D. Duca, T. Potlog, M. Dobromir, V. Nica
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Abstract

CdSe thin films have been prepared by close spaced sublimation technique. The deposited films have been characterized by Scanning Electronic Microscope (SEM), X-ray diffraction (XRD) and X-ray photoelectron spectroscopy (XPS). XRD patterns have been used to determine the microstructural parameters (crystallite size, lattice parameter) of investigated films. Structural investigations showed that studied samples are polycrystalline and have a hexagonal (wurtzite)) structure. Surface morphology studies SEM shows that the nanograins are uniformly distributed over the entire surface and depends on the substrate temperature. The XPS analysis of CdSe thin films indicates the formation on the surface of the CdO oxide.
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近空间升华法制备cdse薄膜的结构和表面研究
采用紧密间隔升华技术制备了CdSe薄膜。采用扫描电镜(SEM)、x射线衍射(XRD)和x射线光电子能谱(XPS)对沉积膜进行了表征。利用XRD谱图测定了所研究薄膜的微观结构参数(晶体尺寸、晶格参数)。结构研究表明,所研究的样品是多晶的,具有六方(纤锌矿)结构。表面形貌研究表明,纳米颗粒均匀分布在整个表面,并与衬底温度有关。CdSe薄膜的XPS分析表明在氧化CdO表面形成。
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