Preparasi Karbon Aktif dari Sabut Kelapa dengan Aktivator Gelombang Mikro untuk Adsorpsi Rhodamin B

Nahdatul Aulia, M. Khair
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引用次数: 1

Abstract

— Activated carbon from coconut husk has been prepared by using microwave assisted activation. Carbonization was conducted at mild condition of 250ºC for 105 minutes heating time. Optimum activated carbon is obtained by using microwave assisted activation at 300 watts of iradiation for 4 minutes contact time with iodine number is 779,7604 mg/g. Characterization of activated carbon using FTIR and proximate analysis (water content, vaporcontent, ash content, bound carbon content and iod absorption). Adsorption test showed that the prepared activated carbon was able to absorp Rhodamin B at the optimum concentration of 200 mg/L. Adsorption isoterm study conducted by Langmuir equation with a regression coefficient R 2 = 0,9640 with a maximum absorption capacity of 2,923 mg/g. FTIR characterization showed that the activated carbon contains a fungsional groups O-H at wave numbers 3600-3200 cm -1 , C=C at wave numbers 1500-1650 cm -1 , and C-O at wave numbers 1300-900 cm -1 .
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椰子壳的活化活化和微波激活器对罗达敏B的适应
用微波辅助活化法制备了椰壳活性炭。炭化在250℃温和条件下进行,加热时间105分钟。采用微波辅助活化法,在300瓦辐照下,接触时间为4分钟,碘值为779、7604 mg/g,得到最佳活性炭。活性炭的表征使用FTIR和近似分析(含水量,汽分,灰分含量,结合碳含量和碘吸收)。吸附试验表明,所制备的活性炭在最佳浓度为200 mg/L时能够吸附罗丹明B。采用Langmuir方程进行吸附等项研究,回归系数r2 = 0.9640,最大吸附量为2923 mg/g。FTIR表征表明,活性炭在波数3600 ~ 3200 cm -1处含有O-H基团,在波数1500 ~ 1650 cm -1处含C=C基团,在波数1300 ~ 900 cm -1处含C- o基团。
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