In-situ-X-ray investigation on vacuum soldering processes for conventional and diffusion soldering

A. Klemm, M. Oppermann, T. Zerna
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引用次数: 3

Abstract

In power electronics there is currently a development to higher operating temperatures of up to 300 °C. This was made possible by an improved availability of semiconductor materials such as silicon carbide. At these temperatures conventional solders can no longer be used for Die-Attachment. Therefore new technologies are necessary. One possible solution is to use diffusion soldering. Khaja et al. [1] presented an approach for diffusion soldering by printing of a conventional solder paste with a 20 μm thin stencil. In power the void content is typically required to be less than 10 %. Khaja et al. showed that the application of a vacuum vapour phase soldering process can ensure a very low void content of the resulting solder joints. In a previous paper we showed that vacuum soldering processes are in principle better suited for this purpose than overpressure processes [2]. In this work we found the same effects, which we observed in our previous work, also for conventional SAC305 solder paste on DCB substrates. Furthermore we investigated different vacuum soldering processes. We could not observe any apparent difference between vacuum soldering processes with several separate vacuum steps and processes with a single vacuum step. However the strength of the vacuum step influences the final void content significantly. Furthermore we found that void content over time curves of soldering processes without pressure changes exhibit a minimum. When a solder joint is kept at peak temperature for a longer period of time the void content steadily increases again. We showed that this can be suppressed with overpressure. Therefore we conclude that for diffusion soldering with long peak times of several minutes a combined soldering process of vacuum and overpressure steps is required.
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传统和扩散真空焊接工艺的现场x射线研究
在电力电子领域,目前正在向高达300°C的更高工作温度发展。这是由于半导体材料如碳化硅的可用性提高而成为可能的。在这样的温度下,传统焊料不能再用于模具连接。因此,新技术是必要的。一种可能的解决方案是使用扩散焊接。Khaja等人[1]提出了一种用20 μm薄的模板打印传统锡膏进行扩散焊接的方法。在电力中,通常要求孔隙含量小于10%。Khaja等人表明,真空气相焊接工艺的应用可以确保所得到的焊点的空隙率非常低。在之前的一篇论文中,我们表明真空焊接工艺原则上比超压工艺更适合于此目的[2]。在这项工作中,我们发现了与我们在之前的工作中观察到的相同的效果,也适用于DCB基板上的传统SAC305锡膏。此外,我们还研究了不同的真空焊接工艺。我们没有观察到有几个单独真空步骤的真空焊接工艺和有一个真空步骤的真空焊接工艺有任何明显的区别。而真空台阶的强度对最终孔隙率影响较大。此外,我们还发现,在没有压力变化的情况下,焊接过程中空洞含量随时间的变化曲线最小。当焊点在峰值温度下保持较长时间时,空洞含量再次稳定增加。我们证明了这可以用超压来抑制。因此,我们得出结论,对于具有几分钟长的峰值时间的扩散焊接,需要真空和超压步骤的组合焊接工艺。
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