Pengaruh Penambahan Cetyltrimethylammonium Bromide (CTAB) pada Silika dari Natrium Silikat (Na2SiO3)

Habibur Rahman Dafnaz, Budhi Oktavia, Hardeli Hardeli, Umar Kalmar Nizar
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引用次数: 2

Abstract

Silica is a useful material in adsorption, electronics, mechanical, medical, art to other fields. In this study, Sodium silicate is used which can be used as a more economical precursor of silica as which is produced from natural silica. Silica was synthesized using the sol-gel method. This study aims to determine the effect of adding CTAB mass and  aging time in synthesizing silica. The synthesized silica was tested for iodine absorption value and characterized using FTIR. Based on the iodine absorption of variations in adding mass CTAB (0,1, 0,15, 0,2, 0,25, and 0,3 gram) and aging time (8, 12, 16, 20 and 24 hours) give the most absorption to optimum conditions of adding mass CTAB at 0,2 gram and aging time at 16 hours. The results of measurements with FTIR showed the presence of absorption bands which indicated the loss of CTAB in the synthesized silica.
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二氧化硅是吸附、电子、机械、医疗、艺术等领域的有用材料。在本研究中,硅酸钠作为二氧化硅的一种更经济的前驱体,由天然二氧化硅生产。采用溶胶-凝胶法合成二氧化硅。本研究旨在确定CTAB添加量和老化时间对合成二氧化硅的影响。对合成的二氧化硅进行了吸碘值测试,并用红外光谱对其进行了表征。根据CTAB添加量(0、1、0、15、0、2、0、25、0、3 g)和陈化时间(8、12、16、20、24 h)的变化,得出CTAB添加量为0、2 g、陈化时间为16 h的最佳条件吸碘量最大。FTIR测量结果表明,合成二氧化硅中存在CTAB损失的吸收带。
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