Evaluation of Asphalt Produced from Waste Tyre and Polyethylene Terephthalate-Based Bitumen with Paraffin Wax as Rejuvenator

David O. Olukanni, Deborah A. Adegoke, Akinbowale A. Akinmejiwa, Daniel E. Bassey, Joel A. Adediran
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Abstract

During pavement construction and rehabilitation, large amounts of bitumen are often required. As such, the need for material diversification in pavement construction is essential to conserve the non-renewable natural resource deposits. This study assessed the use of Polyethylene Terephthalate (PET) waste and grounded tyre combined in varying proportions with aged bitumen modifier, and wax as a rejuvenator in the production of asphaltic concrete. A 10% polymer replacement level was maintained for all modified mix batches with three distinct proportions: 6%-PET:4%-GWT, 5%-PET:5%-GWT, and 4%PET:6%-GWT. The rejuvenator was added in percentages 1, 2, and 3 by the total mass of modified bitumen mix. Results showed that the penetration values of the modified bitumen mixes with wax fall between bitumen grades 20–60, indicating suitability in warmer climates. Ductility results indicate an increase in ductility upon modification compared to the control mix. The 6%PET/4%GWT samples obtained the highest ductility values (M2 = 23.5 cm, M5 = 12.5 cm, M8 = 22 cm, M11 = 24.25 cm). The highest softening point value (84.5°C) was obtained with M3 (5%PET/5%GWT/0%wax). The inclusion of wax as a rejuvenator led to massive increases in viscosity values compared to both the control mix and the mixes without wax. Flash and fire point results fell within the same range, implying that the modification and rejuvenation did not yield significant impact on the flash and fire point properties. Marshall stability results showed that no modified bitumen batch obtained stability up to the control mix. The highest flow value (5.9 mm) was obtained with the M12 (5%PET/5%GWT/3%wax) mix. This was about 47.45% higher than that of the control mix and 23.7% higher than that of the corresponding mix without wax. The study recommends material diversification as well as dosage variation as essential in the drive towards achieving optimum stability in asphaltic composites.
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废轮胎和聚对苯二甲酸乙二醇酯基沥青用石蜡再生剂生产沥青的评价
在路面建设和修复过程中,经常需要大量的沥青。因此,为了保护不可再生的自然资源,铺装施工中材料多样化的需要是必不可少的。本研究评估了在沥青混凝土生产中使用不同比例的聚对苯二甲酸乙二醇酯(PET)废料和磨碎的轮胎与老化的沥青改性剂和蜡作为再生剂。所有改性混合批次均保持10%的聚合物替代水平,其中有三个不同的比例:6%-PET:4%-GWT, 5%-PET:5%-GWT和4%PET:6%-GWT。再生剂按改性沥青混合料总质量的百分比1、2和3添加。结果表明,含蜡改性沥青混合料的渗透值介于20-60沥青等级之间,适合于较温暖的气候条件。延性结果表明,与控制混合料相比,改性后的延性有所增加。6%PET/4%GWT样品的延性值最高(M2 = 23.5 cm, M5 = 12.5 cm, M8 = 22 cm, M11 = 24.25 cm)。M3 (5%PET/5%GWT/0%蜡)的软化点值最高(84.5℃)。与对照混合物和不含蜡的混合物相比,加入蜡作为恢复剂导致粘度值大幅增加。闪点和着火点的结果落在相同的范围内,这意味着改性和年轻化对闪点和着火点的性能没有产生显著的影响。马歇尔稳定性结果表明,改性沥青料的稳定性没有达到对照料的水平。M12 (5%PET/5%GWT/3%wax)的流动值最高,为5.9 mm。这比对照混合物高47.45%,比不加蜡的相应混合物高23.7%。该研究建议,在实现沥青复合材料最佳稳定性的过程中,材料多样化和剂量变化是必不可少的。
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