Study of mechanical properties of indium-based solder alloys for cryogenic applications

IF 1.7 4区 材料科学 Q3 ENGINEERING, ELECTRICAL & ELECTRONIC Soldering & Surface Mount Technology Pub Date : 2022-01-07 DOI:10.1108/ssmt-10-2021-0065
Madhuri Chandrashekhar Deshpande, Rajesh Chaudhari, Ramesh Narayanan, Harishwar Kale
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Abstract

Purpose

This study aims to develop indium-based solders for cryogenic applications.

Design/methodology/approach

This paper aims to investigate mechanical properties of indium-based solder formulations at room temperature (RT, 27 °C) as well as at cryogenic temperature (CT, −196 °C) and subsequently to find out their suitability for cryogenic applications. After developing these alloys, mechanical properties such as tensile and impact strength were measured as per American Society for Testing and Materials standards at RT and at CT. Charpy impact test results were used to find out ductile to brittle transition temperature (DBTT). These properties were also evaluated after thermal cycling (TC) to find out effect of thermal stress. Scanning electron microscope analysis was performed to understand fracture mechanism. Results indicate that amongst the solder alloys that have been studied in this work, In-34Bi solder alloy has the best all-round mechanical properties at RT, CT and after TC.

Findings

It can be concluded from the results of this work that In-34Bi solder alloy has best all-round mechanical properties at RT, CT and after TC and therefore is the most appropriate solder alloy amongst the alloys that have been studied in this work for cryogenic applications

Originality/value

DBTT of indium-based solder alloys has not been found out in the work done so far in this category. DBTT is necessary to decide safe working temperature range of the alloy. Also the effect of TC, which is one of the major reasons of failure, was not studied so far. These parameters are studied in this work.

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低温用铟基钎料合金的力学性能研究
目的开发低温应用的铟基焊料。设计/方法/方法本文旨在研究铟基焊料配方在室温(27°C)和低温(- 196°C)下的机械性能,并随后找出它们在低温应用中的适用性。在开发这些合金之后,按照美国测试和材料协会的标准在RT和CT下测量了拉伸和冲击强度等机械性能。利用夏比冲击试验结果确定了材料的韧脆转变温度。热循环(TC)后对这些性能进行了评价,以找出热应力的影响。通过扫描电镜分析了解断裂机理。结果表明:在所研究的钎料合金中,in - 34bi钎料合金在高温、高温和高温后的综合力学性能最好。从本工作的结果可以得出结论,in - 34bi钎料合金在低温、高温和高温后具有最佳的全面机械性能,因此是本工作所研究的合金中最适合低温应用的钎料合金。迄今为止,在这一类别的工作中尚未发现铟基钎料合金的独创性/价值btt。DBTT是确定合金安全工作温度范围的必要条件。而作为失效的主要原因之一,TC的作用目前尚未得到研究。本文对这些参数进行了研究。
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来源期刊
Soldering & Surface Mount Technology
Soldering & Surface Mount Technology 工程技术-材料科学:综合
CiteScore
4.10
自引率
15.00%
发文量
30
审稿时长
>12 weeks
期刊介绍: Soldering & Surface Mount Technology seeks to make an important contribution to the advancement of research and application within the technical body of knowledge and expertise in this vital area. Soldering & Surface Mount Technology compliments its sister publications; Circuit World and Microelectronics International. The journal covers all aspects of SMT from alloys, pastes and fluxes, to reliability and environmental effects, and is currently providing an important dissemination route for new knowledge on lead-free solders and processes. The journal comprises a multidisciplinary study of the key materials and technologies used to assemble state of the art functional electronic devices. The key focus is on assembling devices and interconnecting components via soldering, whilst also embracing a broad range of related approaches.
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