The Influence of the Phase Arrangement of ATZ Composites on Their Wear Rate Under Ball-on-Disc Tests

M. Grabowy, Agnieszka Wojteczko, Piotr Osada, G. Wiązania, Z. Pędzich
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Abstract

An alumina-toughened zirconia (ATZ) material, fabricated using a procedure consisting of the common sintering of two different zirconia powders, was tested using the ball-on-disc method in a temperature range between 20 and 400 °C. Tetragonal zirconia balls were used as a counterpart. Three different types of microstructure were designed, one consisting in separated alumina inclusions in zirconia matrix, the second one containing alumina inclusion in the amount close to the percolation point and another one which was a combination of two continuous phases, penetrating the whole volume of the composite. It was detected that at elevated temperatures all materials showed distinct decrease of measured wear rate. Composite with a low alumina content showed minimal wear rate at 300 °C and composites with higher amount of alumina were the most wear resistant at 400 °C. There are some evidences that this minimal wear rate is connected with a pseudoplastic behavior of a layer formed between co operating elements of tribological pair.
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ATZ 复合材料的相排列对球盘测试磨损率的影响
一种氧化铝增韧氧化锆(ATZ)材料是通过将两种不同的氧化锆粉末共同烧结的方法制成的,在 20 至 400 ℃ 的温度范围内使用盘上球法对其进行了测试。四角氧化锆球被用作对应物。设计了三种不同类型的微观结构,一种是氧化锆基体中分离的氧化铝夹杂物,另一种是氧化铝夹杂物,其含量接近渗透点,还有一种是两个连续相的组合,渗透到复合材料的整个体积中。研究发现,在温度升高时,所有材料的磨损率都明显下降。氧化铝含量低的复合材料在 300 °C 时磨损率最小,而氧化铝含量高的复合材料在 400 °C 时耐磨性最强。有证据表明,这种最低磨损率与摩擦副中共同工作元素之间形成的层的假塑性行为有关。
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