Mechanism of work hardening and softening behavior of AZ31 magnesium alloy sheets with hard plate accumulative roll bonding

IF 15.8 1区 材料科学 Q1 METALLURGY & METALLURGICAL ENGINEERING Journal of Magnesium and Alloys Pub Date : 2024-11-09 DOI:10.1016/j.jma.2024.10.003
Lu Sun, Feng Li, Jia Yang Zhang, Wen Tao Niu, Mu Zi Cao
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Abstract

In this paper, the work hardening and softening behavior of AZ31 magnesium alloy sheets by hard plate accumulative roll bonding (HP-ARB) process in a specific temperature range was studied for the first time, and the cyclic stress relaxation test, EBSD, TEM and other characterization methods were used. When the rolling temperature is 350 °C, the grain size of magnesium sheets is refined to 4.32 (±0.36) µm on average, and it shows an excellent combination of strength and plasticity. The tensile strength reaches 307 (±8.52) MPa and the elongation is 12.73 (±0.84) %. At this time, the curve of work hardening rate decreases smoothly and the degree of hardening is the lowest, and the amplitude of stress drop Δσp in work softening test is the smallest with the increase of cycle times, which shows that the well coordination between work hardening and softening behavior has been achieved. Research has found that the combined effect of grain boundary strengthening and fine grain strengthening enhances the yield and tensile strength of magnesium sheets after three passes HP-ARB process at 350 °C. This is attributed to the high degree of dislocation slip opening in the pyramidal surface 〈a〉 and 〈c + a〉, which not only coordinates the c-axis strain of the entire grain, but also promotes the slip transfer of dislocations in the fine-grained region, significantly improving the elongation of the sheets. This study provides a new idea for the forming and manufacturing of high performance magnesium alloy sheets.

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硬板累积轧制结合 AZ31 镁合金板材的加工硬化和软化行为机理
本文首次采用硬板累积轧制结合(HP-ARB)工艺研究了 AZ31 镁合金板材在特定温度范围内的加工硬化和软化行为,并采用了循环应力松弛试验、EBSD、TEM 等表征方法。当轧制温度为 350 ℃ 时,镁板的晶粒尺寸平均细化至 4.32 (±0.36) µm,并显示出极佳的强度和塑性组合。拉伸强度达到 307 (±8.52) 兆帕,伸长率为 12.73 (±0.84) %。此时,随着循环次数的增加,加工硬化率曲线平稳下降,硬化程度最低,加工软化试验中的应力下降幅度Δσp最小,这表明加工硬化和软化行为之间实现了良好的协调。研究发现,晶界强化和细晶粒强化的共同作用提高了镁板在 350 °C 下经过三道 HP-ARB 工艺后的屈服强度和抗拉强度。这归功于金字塔形表面〈a〉和〈c + a〉的位错滑移开口度高,不仅协调了整个晶粒的c轴应变,还促进了细晶粒区位错的滑移转移,显著提高了板材的伸长率。这项研究为高性能镁合金板材的成形和制造提供了新思路。
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来源期刊
Journal of Magnesium and Alloys
Journal of Magnesium and Alloys Engineering-Mechanics of Materials
CiteScore
20.20
自引率
14.80%
发文量
52
审稿时长
59 days
期刊介绍: The Journal of Magnesium and Alloys serves as a global platform for both theoretical and experimental studies in magnesium science and engineering. It welcomes submissions investigating various scientific and engineering factors impacting the metallurgy, processing, microstructure, properties, and applications of magnesium and alloys. The journal covers all aspects of magnesium and alloy research, including raw materials, alloy casting, extrusion and deformation, corrosion and surface treatment, joining and machining, simulation and modeling, microstructure evolution and mechanical properties, new alloy development, magnesium-based composites, bio-materials and energy materials, applications, and recycling.
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