Fracture Toughness of Short Fibre-Reinforced Composites-In Vitro Study.

IF 3.1 3区 材料科学 Q3 CHEMISTRY, PHYSICAL Materials Pub Date : 2024-11-02 DOI:10.3390/ma17215368
Noor Kamourieh, Maurice Faigenblum, Robert Blizard, Albert Leung, Peter Fine
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Abstract

The development of dental materials needs to be supported with sound evidence. This in vitro study aimed to measure the fracture toughness of a short fibre-reinforced composite (sFRC), at differing thicknesses. In this study, 2 mm, 3 mm and 4 mm depths of sFRC were prepared. Using ISO4049, each preparation was tested to failure. A total of 60 samples were tested: 10 samples for each combination of sFRC and depth. Fractured samples were viewed, and outcomes were analysed. EXF showed greater toughness than EXP, with a mean of 2.49 (95%CI: 2.25, 2.73) MPa.m1/2 compared to a mean of 2.13 (95%CI: 1.95, 2.31) MPa.m1/2, (F(1,54) = 21.28; p < 0.001). This difference was particularly pronounced at 2 mm depths where the mean (95%CI) values were 2.72 (2.49, 2.95) for EXF and 1.90 (1.78, 2.02) for EXP (Interaction F(2,54) = 7.93; p < 0.001). Both materials performed similarly at the depths of 3 mm and 4 mm. The results for both materials were within the accepted fracture toughness values of dentine of 1.79-3.08 MPa.m1/2. Analysis showed crack deflection and bridging fibre behaviour. The optimal thickness at the cavity base for EXF was 2 mm and for EXP 4 mm. Crack deflection and bridging behaviour indicated that restorations incorporating sFRCs are not prone to catastrophic failure and confirmed that sFRCs have similar fracture toughness to dentine. sFRCs could be a suitable biomimetic material to replace dentine.

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短纤维增强复合材料的断裂韧性--体外研究
牙科材料的开发需要可靠的证据支持。这项体外研究旨在测量不同厚度的短纤维增强复合材料(sFRC)的断裂韧性。在这项研究中,分别制备了 2 毫米、3 毫米和 4 毫米深度的短纤维增强复合材料。使用 ISO4049,对每种制备方法进行了破坏测试。总共测试了 60 个样品:每种 sFRC 和深度组合各 10 个样品。对断裂样品进行了观察和结果分析。EXF 的韧性高于 EXP,平均值为 2.49(95%CI:2.25,2.73)兆帕.m1/2,而 EXP 的平均值为 2.13(95%CI:1.95,2.31)兆帕.m1/2(F(1,54) = 21.28;p < 0.001)。这种差异在 2 毫米深度尤为明显,EXF 的平均值(95%CI)为 2.72 (2.49, 2.95),EXP 为 1.90 (1.78, 2.02)(交互作用 F(2,54) = 7.93; p < 0.001)。两种材料在 3 毫米和 4 毫米深度的表现相似。两种材料的结果都在公认的牙本质断裂韧性值(1.79-3.08 MPa.m1/2)范围内。分析显示了裂纹变形和桥接纤维行为。EXF牙洞底部的最佳厚度为2毫米,EXP牙洞底部的最佳厚度为4毫米。裂纹变形和桥接行为表明,使用 sFRC 的修复体不易发生灾难性破坏,并证实 sFRC 具有与牙本质相似的断裂韧性。
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来源期刊
Materials
Materials MATERIALS SCIENCE, MULTIDISCIPLINARY-
CiteScore
5.80
自引率
14.70%
发文量
7753
审稿时长
1.2 months
期刊介绍: Materials (ISSN 1996-1944) is an open access journal of related scientific research and technology development. It publishes reviews, regular research papers (articles) and short communications. Our aim is to encourage scientists to publish their experimental and theoretical results in as much detail as possible. Therefore, there is no restriction on the length of the papers. The full experimental details must be provided so that the results can be reproduced. Materials provides a forum for publishing papers which advance the in-depth understanding of the relationship between the structure, the properties or the functions of all kinds of materials. Chemical syntheses, chemical structures and mechanical, chemical, electronic, magnetic and optical properties and various applications will be considered.
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