{"title":"Thermal annealing optimization for improved mechanical performance of PLA parts produced via 3D printing","authors":"Çağlar Kahya , Oğuz Tunçel , Onur Çavuşoğlu , Kenan Tüfekci","doi":"10.1016/j.polymertesting.2025.108735","DOIUrl":null,"url":null,"abstract":"<div><div>This study employs an integrated approach using Taguchi, ANOVA, and Grey Relational Analysis to optimize the mechanical performance of PLA parts produced via Fused Filament Fabrication through controlled thermal annealing. The analysis examines the effects of annealing temperature and time on tensile, flexural, compressive, and impact strengths, aiming to identify optimal post-processing conditions for improved material properties. Annealing temperatures ranged from 70 °C to 110 °C, and durations varied between 40 and 200 min. Key findings indicate that the most influential parameters were achieved at 90 °C for 120 min, yielding notable enhancements in tensile strength, flexural strength, compressive strength, and impact resistance. The Taguchi method identified optimal conditions for each mechanical property, with temperature emerging as the most influential factor. ANOVA analysis further quantified the contribution ratio of temperature and time, validating the Taguchi results and confirming that temperature accounted for most of the variation in mechanical performance. Differential Scanning Calorimetry supported these findings, showing increased crystallinity in PLA, thus highlighting the significant impact of optimized thermal annealing on enhancing 3D-printed PLA parts.</div></div>","PeriodicalId":20628,"journal":{"name":"Polymer Testing","volume":"144 ","pages":"Article 108735"},"PeriodicalIF":5.0000,"publicationDate":"2025-02-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Polymer Testing","FirstCategoryId":"88","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0142941825000492","RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"MATERIALS SCIENCE, CHARACTERIZATION & TESTING","Score":null,"Total":0}
引用次数: 0
Abstract
This study employs an integrated approach using Taguchi, ANOVA, and Grey Relational Analysis to optimize the mechanical performance of PLA parts produced via Fused Filament Fabrication through controlled thermal annealing. The analysis examines the effects of annealing temperature and time on tensile, flexural, compressive, and impact strengths, aiming to identify optimal post-processing conditions for improved material properties. Annealing temperatures ranged from 70 °C to 110 °C, and durations varied between 40 and 200 min. Key findings indicate that the most influential parameters were achieved at 90 °C for 120 min, yielding notable enhancements in tensile strength, flexural strength, compressive strength, and impact resistance. The Taguchi method identified optimal conditions for each mechanical property, with temperature emerging as the most influential factor. ANOVA analysis further quantified the contribution ratio of temperature and time, validating the Taguchi results and confirming that temperature accounted for most of the variation in mechanical performance. Differential Scanning Calorimetry supported these findings, showing increased crystallinity in PLA, thus highlighting the significant impact of optimized thermal annealing on enhancing 3D-printed PLA parts.
期刊介绍:
Polymer Testing focuses on the testing, analysis and characterization of polymer materials, including both synthetic and natural or biobased polymers. Novel testing methods and the testing of novel polymeric materials in bulk, solution and dispersion is covered. In addition, we welcome the submission of the testing of polymeric materials for a wide range of applications and industrial products as well as nanoscale characterization.
The scope includes but is not limited to the following main topics:
Novel testing methods and Chemical analysis
• mechanical, thermal, electrical, chemical, imaging, spectroscopy, scattering and rheology
Physical properties and behaviour of novel polymer systems
• nanoscale properties, morphology, transport properties
Degradation and recycling of polymeric materials when combined with novel testing or characterization methods
• degradation, biodegradation, ageing and fire retardancy
Modelling and Simulation work will be only considered when it is linked to new or previously published experimental results.