[Relationship between the infiltration arts and penetration depth of molten glass into aluminum oxide matrix].

Yandong Mu, Yonglie Chao, Yunmao Liao, Yukun Meng
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Abstract

Objective: To explore the influences of infiltration time and temperature on the penetration depth of GI-II glass into alumina matrices, thus providing a theoretical basis for facilitating the clinical fabrication of all-ceramic restorations.

Methods: After preparing cuboid alumina specimens 7 x 7 x 5 mm3 in size, we carried out the infiltration firing procedure at 1100 degrees C for six different time duration (30, 60, 90, 120, 150, 180 minutes), and at five different temperatures (1060, 1080, 1100, 1120, 1140 degrees C) for 1 hour each. The penetration depth of glass into the alumina matrices was measured under a stereoscope with magnification of 10 times.

Results: The infiltration time duration and penetration depth were not linearly but exponentially related for both Vita and GI-II materials (r = 0.9886 for Vita and r = 0.9932 for GI-II). The regression equations were as follows: d2 = 0.1122t - 0.4955 (Vita) and d2 = 0.1638t + 0.5873 (GI-II). The temperature and depth were not linearly related either, with increased penetration speed under higher temperatures for GI-II material; the tendency for Vita material was just the opposite.

Conclusion: At an infiltration temperature of 1100 degrees C, the molten infiltration time duration of GI-II glass could be reduced to 1 hour for copings and 3 hours for anterior bridge substructures due to its better infiltration ability.

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【玻璃熔液渗入氧化铝基体深度与渗透工艺的关系】。
目的:探讨浸润时间和温度对GI-II玻璃进入氧化铝基质渗透深度的影响,为临床制作全瓷修复体提供理论依据。方法:制备尺寸为7 × 7 × 5 mm3的长方体氧化铝样品后,在1100℃下进行6种不同时间(30、60、90、120、150、180分钟)和5种不同温度(1060、1080、1100、1120、1140℃)各1小时的浸润烧制过程。在放大10倍的立体显微镜下测量了玻璃对氧化铝基体的穿透深度。结果:Vita与GI-II材料的浸润时间与渗透深度均不是线性相关,而是指数相关(Vita的r = 0.9886, GI-II的r = 0.9932)。回归方程为:d2 = 0.1122t - 0.4955 (Vita), d2 = 0.1638t + 0.5873 (GI-II)。温度与深度也不呈线性相关,温度越高,GI-II材料的渗透速度越快;Vita材料的趋势正好相反。结论:在1100℃的浸润温度下,由于GI-II玻璃具有较好的浸润能力,其熔融浸润时间可缩短至覆盖层1小时,前桥下层3小时。
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