Daniel J. Colopietro, Julio Pachon, A. Bacon, P. Inglett, Laura Reynolds, C. Rohal
{"title":"Evaluating Methodological Parameters to Quantify Particle Size of Organic Soil Material with Laser Diffraction","authors":"Daniel J. Colopietro, Julio Pachon, A. Bacon, P. Inglett, Laura Reynolds, C. Rohal","doi":"10.1002/saj2.20588","DOIUrl":null,"url":null,"abstract":"The recognition that texture is a “master soil property” points towards the need for actual quantification of particle size in organic soil material. Using a multi‐wave particle size analyzer, fibric and sapric soil samples were circulated in deionized water through a closed aqueous loop at 9.6 L min−1 and the following methodological parameters were investigated: pre‐treatment, circulation time, and refractive index. Our results show that pre‐treatment for organic soil samples is dependent upon the degree of decomposition; the intact and dispersed PSDs for fibrous samples were not different, whereas the PSDs for sapric samples showed a shift from 500 to 2000 (intact) μm to 5 to 100 (dispersed) μm. Circulation time was investigated using mean particle diameter and specific surface area. We demonstrated that as circulation time increased, the mean particle diameter decreased and the specific surface area increased out to 30 minutes as mechanical dispersion and/or the fragmentation of organic particles occurred. However, circulation time after 5 minutes is not significantly different in terms of mean particle diameter. To investigate refractive index, 12 optical models were created. When determined across all intact samples, uncertainty was low within individual bins, with a maximum value of 0.07 ± 0.04% v/v. For dispersed samples, uncertainty increased within the silt sized region and had a maximum value of 0.17 ± 0.07% v/v. This study demonstrates that the particle diameter of organic soil material can be measured by LD with comparable certainty as mineral soil material using the methodological approach in this study.This article is protected by copyright. All rights reserved","PeriodicalId":22142,"journal":{"name":"Soil Science Society of America Journal","volume":null,"pages":null},"PeriodicalIF":2.4000,"publicationDate":"2023-08-25","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Soil Science Society of America Journal","FirstCategoryId":"97","ListUrlMain":"https://doi.org/10.1002/saj2.20588","RegionNum":3,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q2","JCRName":"SOIL SCIENCE","Score":null,"Total":0}
引用次数: 0
Abstract
The recognition that texture is a “master soil property” points towards the need for actual quantification of particle size in organic soil material. Using a multi‐wave particle size analyzer, fibric and sapric soil samples were circulated in deionized water through a closed aqueous loop at 9.6 L min−1 and the following methodological parameters were investigated: pre‐treatment, circulation time, and refractive index. Our results show that pre‐treatment for organic soil samples is dependent upon the degree of decomposition; the intact and dispersed PSDs for fibrous samples were not different, whereas the PSDs for sapric samples showed a shift from 500 to 2000 (intact) μm to 5 to 100 (dispersed) μm. Circulation time was investigated using mean particle diameter and specific surface area. We demonstrated that as circulation time increased, the mean particle diameter decreased and the specific surface area increased out to 30 minutes as mechanical dispersion and/or the fragmentation of organic particles occurred. However, circulation time after 5 minutes is not significantly different in terms of mean particle diameter. To investigate refractive index, 12 optical models were created. When determined across all intact samples, uncertainty was low within individual bins, with a maximum value of 0.07 ± 0.04% v/v. For dispersed samples, uncertainty increased within the silt sized region and had a maximum value of 0.17 ± 0.07% v/v. This study demonstrates that the particle diameter of organic soil material can be measured by LD with comparable certainty as mineral soil material using the methodological approach in this study.This article is protected by copyright. All rights reserved
期刊介绍:
SSSA Journal publishes content on soil physics; hydrology; soil chemistry; soil biology; soil biochemistry; soil fertility; plant nutrition; pedology; soil and water conservation and management; forest, range, and wildland soils; soil and plant analysis; soil mineralogy, wetland soils. The audience is researchers, students, soil scientists, hydrologists, pedologist, geologists, agronomists, arborists, ecologists, engineers, certified practitioners, soil microbiologists, and environmentalists.
The journal publishes original research, issue papers, reviews, notes, comments and letters to the editor, and book reviews. Invitational papers may be published in the journal if accepted by the editorial board.