A. Dandia, Ruby Singh, C. Mérienne, G. Morgant, A. Loupy
{"title":"Solvent-free one-pot synthesis and crystal structure of a spiro[indole-thiazine]","authors":"A. Dandia, Ruby Singh, C. Mérienne, G. Morgant, A. Loupy","doi":"10.1080/02786110310001637617","DOIUrl":null,"url":null,"abstract":"An improved facile one-pot synthesis of 3′-(fluorophenyl)-spiro[3H-indole-3,2′-tetrahydro-1,3-thiazine]-2,4′(1H)-dione is reported using an environmentally friendly green chemistry procedure under microwave irradiation. The crystal structure of the reported compound has been determined by a X-ray diffraction. The molecule is largely planar and has cell parameters of a = 11.181(9) Å, b = 11.06(1) Å, c = 12.715(12) Å, α = 90°, β = 98.31(7)°, γ = 90°.","PeriodicalId":22122,"journal":{"name":"Sulfur Letters","volume":"61 1","pages":"201 - 207"},"PeriodicalIF":0.0000,"publicationDate":"2003-10-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"11","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Sulfur Letters","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1080/02786110310001637617","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 11
Abstract
An improved facile one-pot synthesis of 3′-(fluorophenyl)-spiro[3H-indole-3,2′-tetrahydro-1,3-thiazine]-2,4′(1H)-dione is reported using an environmentally friendly green chemistry procedure under microwave irradiation. The crystal structure of the reported compound has been determined by a X-ray diffraction. The molecule is largely planar and has cell parameters of a = 11.181(9) Å, b = 11.06(1) Å, c = 12.715(12) Å, α = 90°, β = 98.31(7)°, γ = 90°.
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