Solid-state deprotection of dithioacetals using 1-benzyl-4-aza-1-azoniabicyclo[2.2.2]octane periodate

A. Hajipour, A. Ruoho
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引用次数: 2

Abstract

Various dithioacetals have been deprotected to the corresponding carbonyl compounds under solvent-free conditions using 1-benzyl-4-aza-1-azoniabicyclo[2.2.2]octane periodate in the presence of aluminium chloride.
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用1-苄基-4-氮杂-1-氮杂双环[2.2.2]辛烷高碘酸盐固相脱保护二硫缩醛
在无溶剂条件下,在氯化铝存在下,使用1-苄基-4-氮杂化-1-氮烟双环[2.2.2]辛酸盐将各种二硫缩醛脱保护为相应的羰基化合物。
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C-Sulfonyldithioformates as heterodienophiles and enophiles in [4 + 2] cycloaddition and ene reactions Hypervalency in sulfur? ab initio and DFT studies of the structures of thiosulfate and related sulfur oxyanions On the preparation of 3-(5-Formyl-3-thioxo-3H-[1,2]dithiol-4-yl)-propionic acid Solvent-free one-pot synthesis and crystal structure of a spiro[indole-thiazine] Solid-state deprotection of dithioacetals using 1-benzyl-4-aza-1-azoniabicyclo[2.2.2]octane periodate
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