{"title":"A facile synthesis of 4-naphthyl-3-cyano-2-(β-d-pyranosylthio) pyridines","authors":"A. Attia","doi":"10.1080/0278611021000048695","DOIUrl":null,"url":null,"abstract":"The treatment of piperidinium salt of 4-naphthyl-3-cyano-2-thiopyridines with an O -peracetyl-α-D-pyranosyl bromide in dry acetone provides a new and simple method for the synthesis of 2-(β-D-pyranosylthio) pyridines in high yields. The site of glycosylation on the pyridine ring was confirmed by 1 H and 13 C NMR spectral analysis.","PeriodicalId":22122,"journal":{"name":"Sulfur Letters","volume":"26 1","pages":"15 - 9"},"PeriodicalIF":0.0000,"publicationDate":"2003-02-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Sulfur Letters","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1080/0278611021000048695","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 1
Abstract
The treatment of piperidinium salt of 4-naphthyl-3-cyano-2-thiopyridines with an O -peracetyl-α-D-pyranosyl bromide in dry acetone provides a new and simple method for the synthesis of 2-(β-D-pyranosylthio) pyridines in high yields. The site of glycosylation on the pyridine ring was confirmed by 1 H and 13 C NMR spectral analysis.
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