Synthesis and characterization of ZnO, ZnO Doped Ag2O Nanoparticles and its Photocatalytic Activity

B. Sreenivas, N. Chandana, J. Sai Chandra, T. Ch. Anil Kumar, Sumanta Bhattacharya, M. Kalyan Chakravarthi
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Abstract

Zinc oxide (ZnO) nanomaterials play an important role in many industries because of their amazing optical, electrical, mechanical, thermal, and structural capabilities. The current study focuses on the production of ZnO nanoparticles for photocatalytic dye degradation activities, and three types of ZnO nanoparticles are prepared: pure ZnO nanocrystals extracted through chemical and biological route and Ag2O doped ZnO nanoparticles. The average particle size of chemically produced ZnO nanocrystals was predicted to be 34 nm, and SEM examination validated the creation of ZnO nanorods-like structure from chemical technique, which exhibits enhanced photocatalytic activity. X-ray diffraction study of Ag2O/ZnO nanoparticles revealed a hexagonal shape. The average particle size was determined to be between 16 and 17 nm. The findings of the SEM examination also revealed that the produced Ag2O doped ZnO nanoparticles agglomerated in hexagonal forms and adhered as bulks and rods that increased with the amount of Ag nanofluids. As a result, it is determined that agglomerated Ag2O/ZnO nanoparticles with hexagonal and rod structures operate as an efficient photocatalytic agent. It is obvious that 25 ml of Ag2O nanofluid doped with ZnO produces an excellent photocatalyst for organic dye degradation and is appropriate for large-scale applications.
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ZnO、ZnO掺杂Ag2O纳米颗粒的合成、表征及其光催化活性
氧化锌纳米材料以其优异的光学、电学、机械、热学和结构性能在许多工业领域发挥着重要作用。目前的研究重点是制备具有光催化降解染料活性的ZnO纳米颗粒,制备了三种类型的ZnO纳米颗粒:通过化学和生物途径提取的纯ZnO纳米晶体和Ag2O掺杂的ZnO纳米颗粒。化学法制备的ZnO纳米晶体的平均粒径为34 nm, SEM检测证实了化学法制备的ZnO纳米棒状结构具有较强的光催化活性。Ag2O/ZnO纳米颗粒的x射线衍射研究显示其呈六边形。平均粒径在16 ~ 17 nm之间。SEM分析还发现,随着Ag纳米流体的添加量的增加,所制备的Ag2O掺杂ZnO纳米颗粒呈六角形聚集,并呈块状和棒状粘附。结果表明,具有六边形和棒状结构的Ag2O/ZnO纳米颗粒是一种高效的光催化剂。可见,25 ml掺杂ZnO的Ag2O纳米流体是一种很好的降解有机染料的光催化剂,适合大规模应用。
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来源期刊
Current Materials Science
Current Materials Science Materials Science-Materials Science (all)
CiteScore
0.80
自引率
0.00%
发文量
38
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