Pechini溶胶-凝胶法制备Tb3+掺杂Lu3Al5O12薄膜的结构和发光性能

Jian Wang, Siqing Shen, Jianjun Xie, Ying Shi, F. Ai
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引用次数: 0

摘要

采用Pechini溶胶-凝胶法和旋涂技术,在精心清洗的(111)硅片上成功制备了Tb3+掺杂Lu3Al5O12(以下简称LuAG:Tb)薄膜。采用x射线衍射(XRD)、原子力显微镜(AFM)和光致发光(PL)光谱研究了LuAG:Tb薄膜的微观结构和光学性能。XRD结果表明,前驱体膜在900℃左右开始结晶。所有焙烧LuAG:Tb薄膜均呈现Tb3+特征发射带。
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Structure and luminescence properties of Tb3+-doped Lu3Al5O12 films prepared by Pechini sol-gel method
Tb3+-doped Lu3Al5O12(hereinafter referred to as LuAG:Tb) films were successfully prepared by Pechini sol-gel process and spin-coating technique on carefully cleaned (111) silicon wafer. The microstructure and optical properties of the LuAG:Tb films were studied by X-ray diffraction (XRD), atomic force microscopy(AFM), as well as photoluminescence (PL) spectra. The XRD results showed that the precursor films started to crystallize at about 900°C. All as-calcined LuAG:Tb films showed the Tb3+ characteristic emission bands.
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