带静电开关机构的质量分析扫描力显微镜

C. Shao, Y. Kawai, T. Ono, M. Esashi
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摘要

设计、制作了一种飞行时间扫描力显微镜(SFM)探针,并对其性能进行了验证。为了同时实现表面观察和化学分析,对材料表面的化学性质进行成像,该探针通过集成一对静电致动器和弯曲电极,在SFM模式和飞行时间质量分析(TOF-MA)模式之间切换悬臂梁的位置。该机制将应用于在SFM模式下拾取原子或分子,然后通过场蒸发将其发射到TOF质量分析仪,在TOF- ma模式下分析其质量。为了在TOF-MA模式下切换悬臂位置,在180V的驱动电压下,制作的探头在悬臂端产生255¿m的最大位移。利用静电拉入效应,悬臂梁被电极按弯曲形状吸引。悬臂的前缘对准了发射化学物质的集成萃取电极。在SFM模式下,悬臂也被吸引到另一个电极上。在驱动前后,悬臂梁的基频从1.8kHz提高到6.8kHz。计算出的弹簧常数由0.05N/m变为0.34N/m。
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Mass-Analysis Scanning Force Microscopy with Electrostatic Switching Mechanism
A time-of-flight scanning force microscope (SFM) probe with an ability to switch the measurement mode using the electrostatically switching mechanism is designed, fabricated and demonstrated the performance of it. In order to achieve surface observation and chemical analysis simultaneously for imaging the chemical property of a material surface, this probe can switch the positions of the cantilever between SFM mode and time-of-flight mass analysis (TOF-MA) mode by integrating a couple of electrostatic actuator with curved electrode. This mechanism will be applied to pick up an atom or molecule under SFM mode, then emits them to TOF mass analyzer using field evaporation for analyzing its mass in TOF-MA mode. To switch the cantilever position at TOF-MA mode, the fabricated probe generated the 255¿m of maximum displacement at the end of cantilever at an actuation voltage of 180V. The cantilever is attracted with the electrode according to the curved shape using electrostatically pull-in effect. The front edge of the cantilever was aligned in front of integrated extraction electrode for emitting chemical species. In SFM mode, the cantilever was also attracted to another electrode. The fundamental resonant frequency of the cantilever is increased from 1.8kHz to 6.8kHz before and after actuation. A calculated spring constant is changed from 0.05N/m to 0.34N/m.
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