MOD法制备PLZT(8/65/35)薄膜的结构与电学性能

Jianqiang Luo, Weiguo Liu, Shun Zhou, Xiaotao Sun
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引用次数: 0

摘要

采用金属有机分解(MOD)法在Pt(111)/Ti/SiO2/Si(100)衬底上制备了热释电锆钛酸铅镧(PbLa8Zr65Ti35)薄膜。在不同的退火温度和相同的退火时间下,非晶薄膜转变为多晶PLZT薄膜。采用x射线衍射(XRD)和原子力显微镜(AFM)研究了材料的相形成和表面微观结构。XRD数据表明,在650℃时钙钛矿相形成,随着温度升高,焦绿石相抑制。利用敏感势垒层代替其他类型的势垒层制备了PLZT热释电传感器。最后,测量了介质系数和热释电系数。
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Structural and electrical properties of PLZT (8/65/35) thin films prepared by MOD method
Pyroelectric lead lanthanum zirconnate titanate (PbLa8Zr65Ti35) thin films were prepared by a metal-organic decomposition (MOD) method on Pt(111)/Ti/SiO2/Si(100) substrate. After annealing at different temperatures with the same annealing time, the amorphous films were transformed into polycrystalline PLZT films. The phase formation and surface microstructure were investigated by X-ray diffraction (XRD) and atom force microscopy (AFM). The XRD data showed the formation of pervoskite phase at 650°C and indicated suppression of pyrochlore phase as temperature increasing. The PLZT pyroelectric sensor was fabricated based on sensitive barrier layer instead of the other type barrier layer. Finally, dielectric and pyroelectric coefficients was also measured.
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