磁控溅射沉积TiW合金薄膜TCR的研究

Chang-long Cai, Yujia Zhai, Shun Zhou, Huan Liu, Jing Huang, Weiguo Liu
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引用次数: 1

摘要

TiW合金不仅是一种优良的红外辐射材料,而且是一种红外敏感材料,常被用作红外热成像探测器的薄膜。TiW合金薄膜的电阻温度系数(TCR)是影响薄膜性能的重要参数,因此研究TiW合金薄膜沉积参数对TCR的影响是非常必要的。本文采用直流磁控溅射法在普通玻璃上沉积TiW合金薄膜,靶材为高纯TiW合金材料((Ti:W)原子=3:7),工作气体为Ar。采用四点探头计测量不同温度下TiW合金薄膜的方电阻,并根据测量曲线计算TCR。研究了工作压力、Ar流量和溅射电流对TiW合金薄膜TCR的影响。通过研究,得到了最佳工艺参数:溅射电流0.32A,工作压力0.8Pa,氩气流量60sccm。在此条件下,TiW合金薄膜的TCR为2‰/K。测试结果表明,TiW合金薄膜具有良好的时间稳定性。
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Study of TCR of TiW alloy films deposited by magnetron sputtering
TiW alloy is not only a excellent infrared radiant material, but also a infrared sensitive material, and was often used as a film in the infrared thermal imaging detectors. The temperature coefficient of resistance (TCR) of TiW alloy film is an important parameter influencing the characteristic, so it is very necessary to study the effect of TiW alloy films deposition parameters on TCR. In this paper, TiW alloy films were deposited by DC magnetron sputtering on ordinary glass, and the target is high pure TiW alloy material ((Ti:W)atom=3:7), the working gas is Ar. The square resistance of TiW alloy films under the different temperature was measured using four-point probe meter, and TCR was calculated according to the measurement curve. The influence of working pressure, Ar flow rate and sputtering current on the TCR of TiW alloy films was investigated. After studying, the best process parameters were obtained, that are, sputtering current 0.32A, working pressure 0.8Pa, and Ar flow rate 60sccm. Under these condition, TCR of TiW alloy films is 2‰/K. The measurement results indicate that the time stability of TiW alloy films is excellent.
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