中二甲胺修正后的中二甲胺的最佳降解条件

Deni Marlina, Budhi Oktavia, Sri Benti Etika, Syamsi Aini
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摘要

介孔二氧化硅是一种具有2- 50nm孔径的固体二氧化硅。介孔二氧化硅可以固定在表面。二甲胺修饰介孔二氧化硅的目的是修饰胺类化合物。介孔二氧化硅与添加胺类化合物的GPTMS反应后可作为亚硝酸盐阴离子的吸附,采用柱法观察二氧化硅对亚硝酸盐阴离子的吸附,亚硝酸盐阴离子的吸附量为0.0182 mg/g,吸附率为96.71%。然后进行脱附过程,考察其脱附能力的因子为脱附类型,即从吸附的0.0085 mg亚硝酸盐阴离子中释放出0.0071 mg亚硝酸盐阴离子,脱附率为83.52%;最佳浓度因子为0.15M HCl,释放出0.0091 mg亚硝酸盐阴离子,脱附率为100%。
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Penentuan Kondisi Optimum Desorpsi Anion Nitrit Dari Adsorben Silika Mesopori Termodifikasi DMA (Dimethylamine)
Mesoporous silica is a solid silica having a pore size of 2-50 nm. Mesoporous silica can be immobilized to the surface. Modification of mesoporous silica with dimethylamine aims to modify amine compounds. Mesoporous silica with the addition of amine compounds reacted with GPTMS can be used as nitrite anion adsorption to see the absorption of silica to nitrite anions using the column method, the adsorption capacity of nitrite anions is 0.0182 mg/g with an absorption percentage of 96.71%. Then the desorption process was carried out, the factor used to see the desorption ability was the type of desorption, namely hydrochloric acid (HCl) with the release of 0.0071 mg of nitrite anion from 0.0085 mg of nitrite anion that was absorbed and the percentage of desorption was 83.52% and a concentration factor with the optimum concentration of 0.15M HCl with the release of 0.0091 mg of nitrite anion with 100% desorption percentage.
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