A Juliet Christina Mary, M Santhanalakshmi, L Lavanya
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引用次数: 0
摘要
通过简单的共沉淀法合成了焦磷酸镍纳米结构。退火温度影响了 α-Ni2P2O7 晶体结构的形成,并改变了其表面形态。将退火温度从 350 °C 提高到 900 °C,材料的形态分别从不规则的团聚颗粒变为哑铃状的纳米颗粒。在 1 M KOH 电解质溶液中测试了 α-Ni2P2O7 纳米片(NP-2)和哑铃形(NP-3)纳米粒子的电化学性能,在电流密度为 0.8 A g-1 时,它们的最大比电容分别为 146 F g-1 和 121 F g-1。此外,还测试了 NP-2 纳米片对不同致病性革兰氏阳性菌和革兰氏阴性菌的抗菌活性。抑菌区的最高值表明α-Ni2P2O7 纳米片具有良好的抗菌性。
Investigating the electrochemical and antibacterial activities of nickel pyrophosphate [a-Ni2P2O7] nanostructures
Nickel pyrophosphate nanostructures have been synthesized by a simple co-precipitation method. Annealing temperature affected the crystal structure formation of α-Ni2P2O7 and altered the surface morphology. By increasing the annealing temperature from 350 °C to 900 °C, the morphology of the material varies from irregularly shaped agglomerated particles to dumbbell-shaped nanoparticles respectively. The electrochemical performance of α-Ni2P2O7 nanoflakes (NP-2) and dumbbell-shaped (NP-3) nanoparticles is tested at 1 M KOH electrolyte solution, which provides the maximum specific capacitance of 146 and 121 F g−1 at a current density of 0.8 A g−1 respectively. Furthermore, the antibacterial activity of NP-2 nanoflakes is tested against different pathogenic Gram-positive and Gram-negative bacteria. The highest value of the inhibition zone exhibits the good antibiotic nature of the α-Ni2P2O7 nanoflakes.