{"title":"接合温度对瞬态液相接合商业纯钛接头微观结构和机械性能的影响","authors":"Vahid Maleki, Sajad Shakerin, Seyyed Alireza Ziaei, Hamid Omidvar, Seyyed Ehsan Mirsalehi","doi":"10.1007/s11665-023-07813-9","DOIUrl":null,"url":null,"abstract":"<div><p>Commercially pure Ti (AMS 4902) was joined using the transient liquid phase bonding technique. The joining process was implemented at various temperatures of 820, 860, 900, and 1000 °C for 90 min under a vacuum atmosphere of 7.99 Pa. The microstructural investigations were carried out comprehensively using scanning electron microscopy equipped with the EDS elemental detector. The mechanical properties were characterized using the microhardness and shear strength tests. Strength properties in terms of ultimate shear strength and ductility were presented as force-extension diagrams. The presence of eutectic intermetallics in the joint centerline indicated that isothermal solidification was not achieved at low bonding temperatures. However, the increase in temperature to 1000 °C resulted in a fully isothermal solidified joint. The elemental gradients between the bonding centerline and the base metal leveled off at high temperatures of 900 and 1000 °C, where the solubility of Ti increased in the Cu crystal structure. A higher hardness of 270 HV with a uniform gradient was also observed across the joint produced at high temperatures of 900 and 1000 °C. A combination of high strength and ductility was obtained for the samples fabricated at 900 and 1000 °C bonding temperatures.</p></div>","PeriodicalId":644,"journal":{"name":"Journal of Materials Engineering and Performance","volume":"33 9","pages":"4613 - 4619"},"PeriodicalIF":2.2000,"publicationDate":"2024-02-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"The Effect of Bonding Temperature on the Microstructural and Mechanical Properties of Transient Liquid Phase Bonded Commercially Pure Ti Joint\",\"authors\":\"Vahid Maleki, Sajad Shakerin, Seyyed Alireza Ziaei, Hamid Omidvar, Seyyed Ehsan Mirsalehi\",\"doi\":\"10.1007/s11665-023-07813-9\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>Commercially pure Ti (AMS 4902) was joined using the transient liquid phase bonding technique. The joining process was implemented at various temperatures of 820, 860, 900, and 1000 °C for 90 min under a vacuum atmosphere of 7.99 Pa. The microstructural investigations were carried out comprehensively using scanning electron microscopy equipped with the EDS elemental detector. The mechanical properties were characterized using the microhardness and shear strength tests. Strength properties in terms of ultimate shear strength and ductility were presented as force-extension diagrams. The presence of eutectic intermetallics in the joint centerline indicated that isothermal solidification was not achieved at low bonding temperatures. However, the increase in temperature to 1000 °C resulted in a fully isothermal solidified joint. The elemental gradients between the bonding centerline and the base metal leveled off at high temperatures of 900 and 1000 °C, where the solubility of Ti increased in the Cu crystal structure. A higher hardness of 270 HV with a uniform gradient was also observed across the joint produced at high temperatures of 900 and 1000 °C. A combination of high strength and ductility was obtained for the samples fabricated at 900 and 1000 °C bonding temperatures.</p></div>\",\"PeriodicalId\":644,\"journal\":{\"name\":\"Journal of Materials Engineering and Performance\",\"volume\":\"33 9\",\"pages\":\"4613 - 4619\"},\"PeriodicalIF\":2.2000,\"publicationDate\":\"2024-02-20\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Materials Engineering and Performance\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://link.springer.com/article/10.1007/s11665-023-07813-9\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q3\",\"JCRName\":\"MATERIALS SCIENCE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Materials Engineering and Performance","FirstCategoryId":"88","ListUrlMain":"https://link.springer.com/article/10.1007/s11665-023-07813-9","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
The Effect of Bonding Temperature on the Microstructural and Mechanical Properties of Transient Liquid Phase Bonded Commercially Pure Ti Joint
Commercially pure Ti (AMS 4902) was joined using the transient liquid phase bonding technique. The joining process was implemented at various temperatures of 820, 860, 900, and 1000 °C for 90 min under a vacuum atmosphere of 7.99 Pa. The microstructural investigations were carried out comprehensively using scanning electron microscopy equipped with the EDS elemental detector. The mechanical properties were characterized using the microhardness and shear strength tests. Strength properties in terms of ultimate shear strength and ductility were presented as force-extension diagrams. The presence of eutectic intermetallics in the joint centerline indicated that isothermal solidification was not achieved at low bonding temperatures. However, the increase in temperature to 1000 °C resulted in a fully isothermal solidified joint. The elemental gradients between the bonding centerline and the base metal leveled off at high temperatures of 900 and 1000 °C, where the solubility of Ti increased in the Cu crystal structure. A higher hardness of 270 HV with a uniform gradient was also observed across the joint produced at high temperatures of 900 and 1000 °C. A combination of high strength and ductility was obtained for the samples fabricated at 900 and 1000 °C bonding temperatures.
期刊介绍:
ASM International''s Journal of Materials Engineering and Performance focuses on solving day-to-day engineering challenges, particularly those involving components for larger systems. The journal presents a clear understanding of relationships between materials selection, processing, applications and performance.
The Journal of Materials Engineering covers all aspects of materials selection, design, processing, characterization and evaluation, including how to improve materials properties through processes and process control of casting, forming, heat treating, surface modification and coating, and fabrication.
Testing and characterization (including mechanical and physical tests, NDE, metallography, failure analysis, corrosion resistance, chemical analysis, surface characterization, and microanalysis of surfaces, features and fractures), and industrial performance measurement are also covered