基于傅立叶变换的扫描探针显微镜后处理漂移补偿和校准方法

IF 2.1 3区 工程技术 Q2 MICROSCOPY Ultramicroscopy Pub Date : 2024-05-09 DOI:10.1016/j.ultramic.2024.113984
M. Le Ster, S. Pawłowski, I. Lutsyk, P.J. Kowalczyk
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引用次数: 0

摘要

扫描探针显微镜(SPM)在纳米科学中无处不在,它可以观察真实空间中的特征,分辨率可达埃级。扫描探针显微镜的扫描性质是用一个尖锐的探针在表面上进行光栅扫描,其间通过控制反馈回路保持一个物理设定点,这通常意味着图像会受到漂移效应的影响,导致生成的图像失真。虽然有操作中补偿漂移的方法,但校正所获图像中的残余线性漂移往往被忽视。在本文中,我们提出了一种基于倒易空间的技术,用于补偿原子分辨扫描探针显微镜图像中的线性漂移,而无需区分快速和慢速扫描方向;此外,这种方法不需要针对不同扫描方向获得的一组 SPM 图像。相反,晶格参数的先验知识使补偿成为可能。该方法还可用于鉴定和校准 SPM 仪器。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

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Fourier transform-based post-processing drift compensation and calibration method for scanning probe microscopy

Scanning probe microscopy (SPM) is ubiquitous in nanoscale science allowing the observation of features in real space down to the angstrom resolution. The scanning nature of SPM, wherein a sharp tip rasters the surface during which a physical setpoint is maintained via a control feedback loop, often implies that the image is subject to drift effects, leading to distortion of the resulting image. While there are in-operando methods to compensate for the drift, correcting the residual linear drift in obtained images is often neglected. In this paper, we present a reciprocal space-based technique to compensate the linear drift in atomically-resolved scanning probe microscopy images without distinction of the fast and slow scanning directions; furthermore this method does not require the set of SPM images obtained for the different scanning directions. Instead, the compensation is made possible by the a priori knowledge of the lattice parameters. The method can also be used to characterize and calibrate the SPM instrument.

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来源期刊
Ultramicroscopy
Ultramicroscopy 工程技术-显微镜技术
CiteScore
4.60
自引率
13.60%
发文量
117
审稿时长
5.3 months
期刊介绍: Ultramicroscopy is an established journal that provides a forum for the publication of original research papers, invited reviews and rapid communications. The scope of Ultramicroscopy is to describe advances in instrumentation, methods and theory related to all modes of microscopical imaging, diffraction and spectroscopy in the life and physical sciences.
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