利用 GC-IMS 和化学计量学分析蒸制过程中吕梁黑鸡胸肉中的挥发性有机化合物

IF 2.6 3区 农林科学 Q2 FOOD SCIENCE & TECHNOLOGY Journal of Food Quality Pub Date : 2024-05-17 DOI:10.1155/2024/6663167
Linlin He, Rui Chen, Fei Lan, Hui Yang, Ruichang Gao, Wengang Jin
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摘要

清蒸鸡胸肉以其独特的风味和营养价值吸引着人们。本研究首先对蒸制过程中的略阳乌鸡脯肉进行了感官评价,然后通过气相色谱-离子迁移谱(GC-IMS)结合化学计量学对其挥发性有机化合物(VOCs)进行了进一步分析。感官结果表明,蒸煮 15-30 分钟的莱阳乌鸡胸肉在口感、风味和咀嚼感方面更容易接受。共获得 60 个挥发性风味信号峰,定性分析识别出 46 个挥发性有机化合物,其中醛类 24 个(51.19-72.57%),酮类 8 个(10.15-16.97%),醇类 9 个(7.98-13.16%),呋喃类 2 个(2.24-10.85%),酯类 2 个(0.54-1.56%),醚类 1 个(0.05-2.47%)。通过正交偏最小二乘判别分析(OPLS-DA)建立了一个稳定可靠的预测模型,并通过变量在预测中的重要性(VIP>1.0且P<0.05)筛选出18种特征性挥发性有机化合物(包括10种醛、3种醇、3种酮、1种呋喃和1种醚)。主成分分析(PCA)结果表明,累积贡献率为 92%,其中 PC1 和 PC2 的贡献率分别为 68.7% 和 23.3%,这表明这些特征性挥发性有机化合物能很好地判别略阳乌鸡胸脯肉的蒸煮时间。热图聚类分析也显示了类似的区分效果。这些结果可为今后研究、开发和控制略阳乌鸡胸脯肉即食蒸煮产品提供参考。
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Analysis of VOCs in Lueyang Black Chicken Breast Meat during the Steaming Process with GC-IMS and Stoichiometry

Steamed chicken breast meat attracts people for its unique flavor and nutritional benefits. In this study, the sensory evaluation of Lueyang black chicken breast meat during steaming was first performed, and their volatile organic compounds (VOCs) were further analyzed by gas chromatography-ion mobility spectroscopy (GC-IMS) combined with stoichiometry. The sensory results demonstrated that the Lueyang black chicken breast meat steamed for 15–30 min was more acceptable in taste, flavor, and chewiness. A total of 60 volatile flavor signal peaks were obtained, and 46 VOCs were recognized from qualitative analysis, containing 24 aldehydes (51.19–72.57%), 8 ketones (10.15–16.97%), 9 alcohols (7.98-13.16%), 2 furans (2.24–10.85%), 2 esters (0.54–1.56%), and 1 ether (0.05–2.47%). A stable and reliable prediction model was set up by orthogonal partial least squares-discriminant analysis (OPLS-DA), and 18 characteristic VOCs (including 10 aldehydes, 3 alcohols, 3 ketones, 1 furan, and 1 ether) were picked out through variable importance in the projection (VIP>1.0 and p < 0.05). Principal component analysis (PCA) results indicated that the cumulative contribution ratio was 92% with PC1 68.7% and PC2 23.3%, respectively, indicating that these characteristic VOCs could well discriminate the steaming time of Lueyang black chicken breast meat. Heatmap clustering analysis also demonstrated a similar distinguishing effect. These results could provide references for the research, development, and quality control of ready-to-eat steamed products for Lueyang black chicken breast meat in the future.

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来源期刊
Journal of Food Quality
Journal of Food Quality 工程技术-食品科技
CiteScore
5.90
自引率
6.10%
发文量
285
审稿时长
>36 weeks
期刊介绍: Journal of Food Quality is a peer-reviewed, Open Access journal that publishes original research articles as well as review articles related to all aspects of food quality characteristics acceptable to consumers. The journal aims to provide a valuable resource for food scientists, nutritionists, food producers, the public health sector, and governmental and non-governmental agencies with an interest in food quality.
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