ZrO2、TiO2和SiO2纳米颗粒掺入对PMMA义齿基托材料强度和表面性能的比较研究

IF 3 Q3 MATERIALS SCIENCE, BIOMATERIALS International Journal of Biomaterials Pub Date : 2022-04-28 DOI:10.1155/2022/5856545
Emad Azmy, M. R. Al-kholy, Ahmad M. Al-Thobity, M. Gad, M. A. Helal
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引用次数: 12

摘要

目的研究纳米二氧化锆(ZrO2)、二氧化钛(TiO2)和二氧化硅(SiO2)对丙烯酸树脂义齿基托材料抗弯强度、冲击强度、硬度和耐磨性的影响。材料和方法根据美国牙科协会(ADA)每次试验的规格尺寸制作丙烯酸树脂样品。根据纳米填料的不同,将标本分为四组;作为对照,ZrO2 (Z), TiO2, (T)和SiO2 (S)基团。根据纳米颗粒浓度,每组又分为两个亚组;3%和7% (Z3, Z7, T3, T7, S3和S7)。弯曲强度、冲击强度和硬度测量分别采用三点弯曲试验、夏比冲击试验和维氏硬度试验。通过磨损试验前后试样表面粗糙度的差异来测定耐磨性。使用扫描电子显微镜评估纳米颗粒的规格和分布,并进行断口分析。数据分析采用方差分析、Bonferroni事后检验和Kruskal-Wallis检验(α = 0.05)。结果除T7组和S7组(P值<0.001,效应量= 0.893)和(P值<0.001,效应量= 0.759)外,各试验组的抗折和冲击强度均较对照组有显著提高,差异均有统计学意义。除T3、S3组外,各试验组硬度均较对照组有显著提高(P值<0.001,效应量= 0.67)。在磨损方面,除T7和S7组外,所有测试组的耐磨性均有统计学意义的增强(P值<0.001,效应值= 0.685)。结论ZrO2浓度和低TiO2、SiO2浓度均能提高材料的抗弯强度、冲击强度和耐磨性。随着ZrO2浓度的增加以及TiO2和SiO2浓度的增加,材料的硬度均有所增加。
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Comparative Effect of Incorporation of ZrO2, TiO2, and SiO2 Nanoparticles on the Strength and Surface Properties of PMMA Denture Base Material: An In Vitro Study
Objective This study aimed to investigate the effects of nanoparticles (zirconium dioxide (ZrO2), titanium dioxide (TiO2), and silicon dioxide (SiO2)) on the flexural strength, impact strength, hardness, and wear resistance of the acrylic resin denture base material. Materials and Methods Acrylic resin specimens were fabricated in dimensions according to American Dental Association (ADA) specifications per test. Specimens were divided according to nanofiller into four groups; unmodified as control, ZrO2 (Z), TiO2, (T), and SiO2 (S) groups. Each one was subdivided into two subgroups according to nanoparticle concentrations; 3% and 7% (Z3, Z7, T3, T7, S3, and S7). A 3-point bending test, Charpy impact test, and Vickers hardness test were used for flexural strength, impact strength, and hardness measurements, respectively. Wear resistance was measured by the differences in surface roughness of tested specimens before and after the wear test. A scanning electron microscope was used to assess nanoparticle specifications and distributions and for fracture surfaces analysis. ANOVA, Bonferroni's post hoc test, and the Kruskal–Wallis test were applied for data analysis (α = 0.05). Results Regarding the flexural and impact strength, there was a statistically remarkable increase for all tested groups compared with the control group, except for the T7 and S7 groups (P value <0.001, effect size = 0.893) and (P value <0.001, effect size = 0.759), respectively. There was a statistically significant improvement in the hardness of all tested groups compared with the control group (P value <0.001, effect size = 0.67) except T3 and S3. Regarding wear, a statistically significant enhancement was noticed in the wear resistance of all tested groups (P value <0.001, effect size = 0.685), except for the T7 and S7 groups. Conclusion The flexural strength, impact strength, and wear resistance improved with both concentrations of ZrO2 and low TiO2 and SiO2 concentrations. The hardness increased with both concentrations of ZrO2 and high TiO2 and SiO2 concentrations.
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来源期刊
International Journal of Biomaterials
International Journal of Biomaterials MATERIALS SCIENCE, BIOMATERIALS-
CiteScore
4.30
自引率
3.20%
发文量
50
审稿时长
21 weeks
期刊最新文献
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